1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride

Base Information

Chemical Name:1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride
CAS No.:85620-36-6
Molecular Formula:C9H13ClO
Molecular Weight:172.65200
Hs Code.:2916209090
DSSTox Substance ID:DTXSID40510592
Mol file:85620-36-6.mol

Synonyms:85620-36-6;1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride;DTXSID40510592

Suppliers and Price of 1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:2.88830
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:172.0654927
Heavy Atom Count:11
Complexity:198

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCCCC1=C)C(=O)Cl

Technology Process of 1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride

There total 4 articles about 1-Methyl-2-methylidenecyclohexane-1-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 49716-75-8
1-methyl-2-methyliden-1-cyclohexancarbonsaeure

: 85620-36-6
1-methyl-2-methylen-1-cyclohexancarbonsaeurechlorid

Guidance literature:: With thionyl chloride; at 120 ℃; for 0.833333h;
DOI:10.1002/hlca.19840670110

Reference yield:

: 66088-37-7,5453-94-1
ethyl 1-methyl-2-oxocyclohexancarboxylate

: 85620-36-6
1-methyl-2-methylen-1-cyclohexancarbonsaeurechlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / tetrahydrofuran / 2 h / Ambient temperature

2: 90 percent / KOH / methanol / 24 h / Heating

3: 98 percent / SOCl₂ / 0.83 h / 120 °C

With potassium hydroxide; thionyl chloride; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19840670110

Reference yield:

: 49673-60-1
1-methyl-2-methylen-1-cyclohexancarbonsaeure-aethylester

: 85620-36-6
1-methyl-2-methylen-1-cyclohexancarbonsaeurechlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / KOH / methanol / 24 h / Heating

2: 98 percent / SOCl₂ / 0.83 h / 120 °C

With potassium hydroxide; thionyl chloride; In methanol;
DOI:10.1002/hlca.19840670110