Bicyclo(3.3.1)non-3-en-2-one

Base Information

Chemical Name:Bicyclo(3.3.1)non-3-en-2-one
CAS No.:10036-12-1
Molecular Formula:C9H12 O
Molecular Weight:0
Hs Code.:2914299000
DSSTox Substance ID:DTXSID90143233
Mol file:10036-12-1.mol

Synonyms:10036-12-1;BICYCLO[3.2.2]NON-3-EN-2-ONE;bicyclo[3.2.2]non-2-en-4-one;SCHEMBL6470587;DTXSID90143233

Suppliers and Price of Bicyclo(3.3.1)non-3-en-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Bicyclo(3.3.1)non-3-en-2-one

Chemical Property:

Vapor Pressure:0.0559mmHg at 25°C
Boiling Point:233.4°Cat760mmHg
Flash Point:102°C
PSA：17.07000
Density:1.043g/cm³
LogP:1.93170
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:136.088815002
Heavy Atom Count:10
Complexity:173

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2CCC1C=CC2=O

Technology Process of Bicyclo(3.3.1)non-3-en-2-one

There total 10 articles about Bicyclo(3.3.1)non-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 57807-62-2
3-bromobicyclo<3.3.1>nonan-2-one

: 10036-12-1
bicyclo<3.3.1>non-3-en-2-one

Guidance literature:: With lithium carbonate; lithium bromide; In N,N-dimethyl-formamide; at 110 ℃; for 5h;
DOI:10.1246/bcsj.60.4369

Reference yield: 62.0%

: Acetic acid 4-bromo-bicyclo[3.3.1]non-2-en-2-yl ester

: 10036-12-1
bicyclo<3.3.1>non-3-en-2-one

Guidance literature:: With hydrogenchloride; In ethanol; at 70 ℃; for 1h;

Reference yield:

: 2568-17-4
bicyclo[3.3.1]nonan-2-one

: 10036-12-1
bicyclo<3.3.1>non-3-en-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / phenyltrimethylammonium tribromide / tetrahydrofuran / 0.5 h / 0 °C

2: 95 percent / LiBr, Li₂CO₃ / dimethylformamide / 5 h / 110 °C

With phenyltrimethylammonium tribromide; lithium carbonate; lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.60.4369