(2,6-dichlorophenyl)methanesulfonyl chloride

Base Information

• Chemical Name: (2,6-dichlorophenyl)methanesulfonyl chloride
• CAS No.: 85952-31-4
• Molecular Formula: C7H5Cl3O2S
• Molecular Weight: 259.541
• Hs Code.: 2904909090
• Mol file: 85952-31-4.mol

Synonyms:2,6-Dichlorobenzylsulfonyl chloride;2,6-dichlorophenylmethanesulfonyl chloride;2,6-dichlorobenzylsulphonyl chloride;

Chemical Property of (2,6-dichlorophenyl)methanesulfonyl chloride

Chemical Property:

• PSA: 42.52000
• LogP: 4.14280

Purity/Quality:

97% ^*data from raw suppliers

(2,6-Dichlorophenyl)methanesulfonyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,6-dichlorophenyl)methanesulfonyl chloride

There total 4 articles about (2,6-dichlorophenyl)methanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(2,6-dichlorobenzylthio)-acetic acid (65051-35-6) → 2,6-dichlorobenzylsulphonyl chloride (85952-31-4)

Guidance literature:

With sodium acetate; chlorine; In water; acetic acid;

Reference yield: 53.0%

→ 2,6-dichlorobenzylsulphonyl chloride (85952-31-4)

Guidance literature:

Reference yield:

sodium (2,6-dichloro-phenyl)-methanesulfonic acid (1154613-75-8) → 2,6-dichlorobenzylsulphonyl chloride (85952-31-4)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; at 5 - 20 ℃;

DOI:10.1002/ejoc.201200670

upstream raw materials:

1,3-Dichloro-2-chloromethyl-benzene

(2,6-dichlorobenzylthio)-acetic acid

sodium (2,6-dichloro-phenyl)-methanesulfonic acid

Downstream raw materials:

1-(2,6-dichlorophenyl)-3-(4-methoxyphenyl)-2-thia-3-azabicyclo[3.1.0]hexane 2,2-dioxide

N-allyl-1-(2,6-dichlorophenyl)-N-(4-methoxyphenyl)methanesulfonamide

2,6-dichlorobenzylsulfonamide

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