9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-

Base Information

Chemical Name:9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-
CAS No.:86456-19-1
Molecular Formula:C26H28N2O5S
Molecular Weight:480.5759
Hs Code.:
NSC Number:355186
UNII:46TJ5VZX8Q
DSSTox Substance ID:DTXSID90235566
Wikidata:Q83117447

Synonyms:86456-19-1;9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-;NSC355186;NSC 355186;NSC-355186;9H-Xanthen-9-one, 1-[[2-(diethylamino)ethyl]amino]-7-[[(4-methylphenyl)sulfonyl]oxy]-;46TJ5VZX8Q;DTXSID90235566;[8-(2-diethylaminoethylamino)-9-oxo-xanthen-2-yl] 4-methylbenzenesulfonate;1-[[2-(Diethylamino)ethyl]amino]-7-[[(4-methylphenyl)sulfonyl]oxy]-9H-xanthen-9-one;8-{[2-(DIETHYLAMINO)ETHYL]AMINO}-9-OXO-9H-XANTHEN-2-YL 4-METHYLBENZENE-1-SULFONATE

Suppliers and Price of 9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-

Chemical Property:

Vapor Pressure:1.22E-17mmHg at 25°C
Boiling Point:666.7°Cat760mmHg
Flash Point:357°C
Density:1.289g/cm³
XLogP3:5.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:9
Exact Mass:480.17189317
Heavy Atom Count:34
Complexity:773

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CCNC1=C2C(=CC=C1)OC3=C(C2=O)C=C(C=C3)OS(=O)(=O)C4=CC=C(C=C4)C

Technology Process of 9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)-

There total 5 articles about 9H-Xanthen-9-one, 1-((2-(diethylamino)ethyl)amino)-7-(((4-methylphenyl)sulfonyl)oxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 86456-17-9
1-<<2-(diethylamino)ethyl>amino>-7-hydroxy-9H-xanthen-9-one

: 98-59-9
p-toluenesulfonyl chloride

: 86456-19-1
1-<<2-(diethylamino)ethyl>amino>-7-(toluenesulfonyloxy)-9H-xanthen-9-one

Guidance literature:: With pyridine; at 50 ℃; for 1.5h;
DOI:10.1021/jm00363a007

Reference yield:

: 625-99-0
3-iodochlorobenzene

: 86456-19-1
1-<<2-(diethylamino)ethyl>amino>-7-(toluenesulfonyloxy)-9H-xanthen-9-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) K₂CO₃, 2.) Cu, CuI / 1.) DMF, 120 deg C, 10 min, 2.) DMF, reflux, 50 h

2: 1.) 50percent polyphosphoric acid, 2.) pyridine / 1.) 120 deg C, 3 h, 2.) reflux, 16 h

3: 86 percent / 56percent HI / 4 h / Heating

4: 85 percent / pyridine / 1.5 h / 50 °C

With pyridine; copper(l) iodide; PPA; hydrogen iodide; copper; potassium carbonate;
DOI:10.1021/jm00363a007

Reference yield:

: 2612-02-4
5-methoxysalicylic acid

: 86456-19-1
1-<<2-(diethylamino)ethyl>amino>-7-(toluenesulfonyloxy)-9H-xanthen-9-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) K₂CO₃, 2.) Cu, CuI / 1.) DMF, 120 deg C, 10 min, 2.) DMF, reflux, 50 h

2: 1.) 50percent polyphosphoric acid, 2.) pyridine / 1.) 120 deg C, 3 h, 2.) reflux, 16 h

3: 86 percent / 56percent HI / 4 h / Heating

4: 85 percent / pyridine / 1.5 h / 50 °C

With pyridine; copper(l) iodide; PPA; hydrogen iodide; copper; potassium carbonate;
DOI:10.1021/jm00363a007