4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol

Base Information

• Chemical Name: 4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol
• CAS No.: 86120-46-9
• Molecular Formula: C10H20O2Si
• Molecular Weight: 200.353
• DSSTox Substance ID: DTXSID80420141
• Nikkaji Number: J435.904F
• Wikidata: Q82231361

Synonyms:86120-46-9;4-[tert-butyl(dimethyl)silyl]oxybut-2-yn-1-ol;4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol;4-[(TERT-BUTYLDIMETHYLSILYL)OXY]BUT-2-YN-1-OL;2-Butyn-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-;4-((tert-butyldimethylsilyl)oxy)but-2-yn-1-ol;UPCMLD00WV-89;SCHEMBL2749023;DTXSID80420141;TVWVWXDQNWGYJZ-UHFFFAOYSA-N;MFCD29042410;AKOS037643975;AS-43693;4-(tert-Butyldimethylsiloxy)-2-butyn-1-ol;4-tert-Butyldimethylsilyloxy-but-2-in-1-ol;1-(tert-butyldimethylsilyloxy)but-2-yn-4-ol;4-((t-Butyldimethylsilyl)oxy)but-2-yn-1-ol;EN300-253739;4-(tert-butyl-dimethylsilanyloxy)-but-2-yne-1-ol;4-{[tert-butyl(dimethyl)silyl]oxy}but-2-yn-1-ol;A1-31439

Chemical Property of 4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 200.123256411
• Heavy Atom Count: 13
• Complexity: 214

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C)(C)[Si](C)(C)OCC#CCO

Technology Process of 4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol

There total 1 articles about 4-(tert-Butyl-dimethyl-silanyloxy)-but-2-yn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-tert-butyldimethylsilyloxy-4-triethylsilyloxy-2-butyne → 1,4-dihydroxybut-2-yne (110-65-6) + 4-(tert-butyldimethylsilyloxy)-2-butyn-1-ol (86120-46-9)

Guidance literature:

With MCM-41; In methanol; for 4h; Ambient temperature;

Reference yield: 99.0%

2-nitro-N-(prop-2-yn-1-yl)benzene-1-sulfonamide (908072-33-3) + 4-(tert-butyldimethylsilyloxy)-2-butyn-1-ol (86120-46-9) → N-[4-(tert-butyldimethylsilyloxy)but-2-ynyl]-N-(prop-2-ynyl)-2-nitrophenylsulfonamide

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; for 12h;

DOI:10.1002/ejoc.201403535

Reference yield: 94.0%

4-methyl-N-prop-2-ynylbenzenesulfonamide (55022-46-3) + 4-(tert-butyldimethylsilyloxy)-2-butyn-1-ol (86120-46-9) → N-[4-(tert-butyldimethylsilyloxy)but-2-ynyl]-N-(prop-2-ynyl)-4-methylphenylsulfonamide

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; for 12h;

DOI:10.1002/ejoc.201403535

Downstream raw materials:

2,3-butadien-1-ol

1-[2-(4-tert-butyldimethylsilyloxy-2-butynyloxy)-3-methylphenyl]ethanone

(Z)-4-(tert-butyldimethylsiloxy)-3-phenylbut-2-en-1-ol

4-[(tert-butyldimethylsilyl)oxy]but-2-yn-1-yl 4-methylbenzene-1-sulfonate

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