N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine

Base Information

Chemical Name:N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine
CAS No.:86140-67-2
Molecular Formula:C9H14N2S
Molecular Weight:182.29
Hs Code.:
DSSTox Substance ID:DTXSID80707222
Nikkaji Number:J2.050.677F
Wikidata:Q82640912

Synonyms:86140-67-2;N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine;SCHEMBL13236108;DTXSID80707222;N-(o-methylthiophenyl)ethylenediamine;N-[2-(Methylthio)phenyl]ethylenediamine

Suppliers and Price of N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:182.08776963
Heavy Atom Count:12
Complexity:119

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC1=CC=CC=C1NCCN

Technology Process of N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine

There total 4 articles about N~1~-[2-(Methylsulfanyl)phenyl]ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 169281-35-0
2-amino-N-(2-methylsulfanyl-phenyl)-acetamide

: 86140-67-2
1-Amino-2-N-[2-(methylthio)phenyl]aminoethane

Guidance literature:: With borane-THF; for 18h; Heating;

Reference yield: 40.0%

: 63934-53-2
2-(methylthio)aniline hydrochloride

: 2987-53-3
2-(Methylthio)aniline

: 86140-67-2
1-Amino-2-N-[2-(methylthio)phenyl]aminoethane

Guidance literature:: With formaldehyd; In methanol; water;

Reference yield:

: 2987-53-3
2-(Methylthio)aniline

: 86140-67-2
1-Amino-2-N-[2-(methylthio)phenyl]aminoethane

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / DMAP / acetonitrile / 6 h / Heating

2: 92 percent / TFA / 1 h / 20 °C

3: 81 percent / BH₃*THF / 18 h / Heating

With dmap; borane-THF; trifluoroacetic acid; In acetonitrile;