1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-

Base Information

Chemical Name:1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-
CAS No.:862587-60-8
Molecular Formula:C20H35NO4
Molecular Weight:353.49600
Hs Code.:
DSSTox Substance ID:DTXSID10463566
Wikidata:Q82288502

Synonyms:1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-;862587-60-8;DTXSID10463566

Suppliers and Price of 1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-

Chemical Property:

Boiling Point:526.2±45.0 °C(Predicted)
PSA：68.12000
Density:1.05±0.1 g/cm3(Predicted)
LogP:4.72850
XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:11
Exact Mass:353.25660860
Heavy Atom Count:25
Complexity:418

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCC1(OCCO1)CC(=O)NC2CCCCC2=O
Isomeric SMILES:CCCCCCCCCC1(OCCO1)CC(=O)N[C@H]2CCCCC2=O

Technology Process of 1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]-

There total 8 articles about 1,3-Dioxolane-2-acetamide, 2-nonyl-N-[(1S)-2-oxocyclohexyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: N-(2-hydroxy-cyclohexyl)-2-(2-nonyl-[1,3]dioxolan-2-yl)-acetamide

: 862587-60-8
2-(2-nonyl-[1,3]dioxolan-2-yl)-N-(2-oxo-cyclohexyl)-acetamide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/b412802h

Reference yield: 58.0%

: trans-N-(2-hydroxy-cyclohexyl)-2-(2-nonyl-[1,3]dioxolan-2-yl)-acetamide

: 862587-60-8
2-(2-nonyl-[1,3]dioxolan-2-yl)-N-(2-oxo-cyclohexyl)-acetamide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 25 ℃;
DOI:10.1039/b412802h

Reference yield:

: 109873-29-2
(2-nonyl-[1,3]dioxolan-2-yl)-acetic acid methyl ester

: 862587-60-8
2-(2-nonyl-[1,3]dioxolan-2-yl)-N-(2-oxo-cyclohexyl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / aq. NaOH / 3 h

2: 100 percent / ClOCCOCl; DMF / CH₂Cl₂ / 120 h / 0 °C

3: 60 percent / aq. NaHCO₃ / CH₂Cl₂

4: 58 percent / PCC / CH₂Cl₂ / 4 h / 20 °C

With sodium hydroxide; oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; pyridinium chlorochromate; In dichloromethane;
DOI:10.1039/b412802h