(6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester

Base Information

Chemical Name:(6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester
CAS No.:862822-06-8
Molecular Formula:C12H13N3O4S
Molecular Weight:295.31400
Hs Code.:
Mol file:862822-06-8.mol

Synonyms:6-Nitro-benzothiazol-2-carbonsaeure;6-nitro-benzothiazole-2-carboxylic acid;6-nitrobenzothiazol-2-yl tert-butyl carbamate;

Suppliers and Price of (6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(6-nitrobenzo[d]thiazol-2-yl)carbamate 97%
5g
$ 677.00

Chemcia Scientific
(6-Nitro-benzothiazol-2-yl)-carbamicacidtert-butylester ＞97%
5 G
$ 795.00

Total 2 raw suppliers

Chemical Property of (6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester

Chemical Property:

PSA：128.77000
LogP:4.08830

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl(6-nitrobenzo[d]thiazol-2-yl)carbamate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester

There total 1 articles about (6-Nitro-benzothiazol-2-yl)-carbaMic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6285-57-0
2-amino-6-nitrobenzothiazole

: 24424-99-5
di-tert-butyl dicarbonate

: 862822-06-8
(6-nitrobenzothiazol-2-yl)carbamic acid tert-butyl ester

Guidance literature:: With dmap; In dichloromethane; at 25 ℃; for 18h;
DOI:10.1016/j.bmcl.2005.05.077

Reference yield:

: 862822-06-8
(6-nitrobenzothiazol-2-yl)carbamic acid tert-butyl ester

: 2,6-dichloro-N-[2-(3-hexyl-ureido)-benzothiazol-6-yl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / H₂ / Pd/C / tetrahydrofuran / 13 h / 25 °C

2: 93 percent / N,N-dimethyl-acetamide / 20 h / 25 °C

3: 92 percent / HCl / dioxane; ethanol / 17 h / 25 °C

4: 45 percent / pyridine / 16 h / 60 °C

With pyridine; hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2005.05.077

Reference yield:

: 862822-06-8
(6-nitrobenzothiazol-2-yl)carbamic acid tert-butyl ester

: 2,6-dichloro-N-[2-(3-ethyl-ureido)-benzothiazol-6-yl]-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / H₂ / Pd/C / tetrahydrofuran / 13 h / 25 °C

2: 93 percent / N,N-dimethyl-acetamide / 20 h / 25 °C

3: 92 percent / HCl / dioxane; ethanol / 17 h / 25 °C

4: 50 percent / pyridine / 16 h / 60 °C

With pyridine; hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2005.05.077