3,4-Dimethoxyphenyltributyltin

Base Information

Chemical Name:3,4-Dimethoxyphenyltributyltin
CAS No.:86487-18-5
Molecular Formula:C20H36O2Sn
Molecular Weight:427.215
Hs Code.:
DSSTox Substance ID:DTXSID101287464

Synonyms:SCHEMBL246540;3,4-dimethoxyphenyltributyltin;CCSCCVLBMDKDBP-UHFFFAOYSA-N;DTXSID101287464;Tributyl(3,4-dimethoxyphenyl)stannane;86487-18-5

Suppliers and Price of 3,4-Dimethoxyphenyltributyltin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Dimethoxyphenyltributyltin

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:12
Exact Mass:428.173733
Heavy Atom Count:23
Complexity:274

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CC(=C(C=C1)OC)OC

Technology Process of 3,4-Dimethoxyphenyltributyltin

There total 2 articles about 3,4-Dimethoxyphenyltributyltin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.1%

: 2859-78-1
4-Bromoveratrole

: 813-19-4
bis(tri-n-butyltin)

: 86487-18-5
tri-n-butyl(3,4-dimethoxyphenyl)stannane

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 120 ℃; for 48h; Inert atmosphere;

Reference yield: 63.0%

: 2859-78-1
4-Bromoveratrole

: 1461-22-9
tributyltin chloride

: 86487-18-5
tri-n-butyl(3,4-dimethoxyphenyl)stannane

Guidance literature:: With phenyllithium; In tetrahydrofuran; byproducts: 3,3',4,4'-tetramethoxybiphenyl; BuLi in hexane, then Bu3SnCl added to dry soln. of 4-bromoveratrole under N2 at -78°C;; saturated NH4Cl soln. added; extd. with ether; washed with brine; dried (Na2SO4); solvent removed; tetramethoxybiphenyl pptd. from light petroleum; main product isolated by distn.; elem. anal.;;