1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-

Base Information

Chemical Name:1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-
CAS No.:865541-38-4
Molecular Formula:C16H16O5S
Molecular Weight:320.366
Hs Code.:
ChEMBL ID:CHEMBL204465
DSSTox Substance ID:DTXSID00460680
Nikkaji Number:J2.394.721H

Synonyms:1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-;865541-38-4;CHEMBL204465;DTXSID00460680

Suppliers and Price of 1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:320.07184478
Heavy Atom Count:22
Complexity:368

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC2=C(C(=C1)OC)SCC(O2)C3=CC(=C(C=C3)O)O

Technology Process of 1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)-

There total 3 articles about 1,2-Benzenediol, 4-(2,3-dihydro-5,7-dimethoxy-1,4-benzoxathiin-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 865541-38-4
4-(5,7-dimethoxy-2,3-dihydro-benzo[1,4]oxathiin-2-yl)-benzene-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 20 °C

2: 29 percent / Et₃N / CHCl₃ / 60 °C

3: 83 percent / TBAF*3H₂O / tetrahydrofuran / 0 °C

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; chloroform; 2: hetero Diels-Alder reaction;
DOI:10.1039/b507496g

Reference yield:

: 342646-87-1
2-(2-hydroxy-4,6-dimethoxy-phenylsulfanyl)-isoindole-1,3-dione

: 865541-38-4
4-(5,7-dimethoxy-2,3-dihydro-benzo[1,4]oxathiin-2-yl)-benzene-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / Et₃N / CHCl₃ / 60 °C

2: 83 percent / TBAF*3H₂O / tetrahydrofuran / 0 °C

With tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; chloroform; 1: hetero Diels-Alder reaction;
DOI:10.1039/b507496g