methyl 3-iodo-4-(N-methylanilino)benzoate

Base Information

Chemical Name:methyl 3-iodo-4-(N-methylanilino)benzoate
CAS No.:868540-78-7
Molecular Formula:C15H14INO2
Molecular Weight:367.186
Hs Code.:
DSSTox Substance ID:DTXSID101262179
Nikkaji Number:J2.278.301G

Synonyms:868540-78-7;DTXSID101262179;Methyl 3-iodo-4-(methylphenylamino)benzoate

Suppliers and Price of methyl 3-iodo-4-(N-methylanilino)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-iodo-4-(N-methylanilino)benzoate

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:367.00693
Heavy Atom Count:19
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=CC=C1)C2=C(C=C(C=C2)C(=O)OC)I

Technology Process of methyl 3-iodo-4-(N-methylanilino)benzoate

There total 1 articles about methyl 3-iodo-4-(N-methylanilino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 868540-77-6
methyl 3-iodo-4-(methylamino)benzoate

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 868540-78-7
methyl 3-iodo-4-[methyl(phenyl)amino]benzoate

Guidance literature:: With cesium fluoride; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1021/jo051549p

Reference yield: 84.0%

: 868540-78-7
methyl 3-iodo-4-[methyl(phenyl)amino]benzoate

: 536-74-3
phenylacetylene

: 868540-86-7
methyl 4-[methyl(phenyl)amino]-3-(phenylethynyl)benzoate

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; at 20 ℃; for 24h;
DOI:10.1021/jo051549p

Reference yield:

: 868540-78-7
methyl 3-iodo-4-[methyl(phenyl)amino]benzoate

: methyl 3-iodo-1,2-diphenylindole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Et₃N; CuI / PdCl₂(PPh₃)2 / 24 h / 20 °C

2: 80 percent / I₂ / CH₂Cl₂ / 1 h / 20 °C

With copper(l) iodide; iodine; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; 1: Sonogashira coupling;
DOI:10.1021/jo051549p