1H-Imidazole, 2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl]-

Base Information

Chemical Name:1H-Imidazole, 2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl]-
CAS No.:86921-46-2
Molecular Formula:C20H22N2O
Molecular Weight:306.40100
Hs Code.:

Synonyms:1-<(p-Benzyloxy)phenethyl>-2,4-dimethylimidazole;2,4-dimethyl-1-<2-<4-(phenylmethoxy)phenyl>ethyl>-1H-imidazole;1H-Imidazole,2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl];

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Imidazole, 2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl]-

Chemical Property:

PSA：27.05000
LogP:4.32160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Imidazole, 2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl]-

There total 1 articles about 1H-Imidazole, 2,4-dimethyl-1-[2-[4-(phenylmethoxy)phenyl]ethyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 592-20-1
Acetol acetate

: 86587-62-4
2-(4'-benzyloxy)phenethyl-p-methylbenzenesulfonate

: 75-07-0,9002-91-9
acetaldehyde

: 1-<(p-Benzyloxy)phenethyl>-2,5-dimethylimidazole

: 86921-46-2
2,4-dimethyl-1-<2-<4-(phenylmethoxy)phenyl>ethyl>-1H-imidazole

Guidance literature:: With ammonium hydroxide; copper diacetate; sodium hydride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) 0 - 100 deg C, 15 - 20 min, 2.) THF, 2 h;
DOI:10.1021/jo00169a027

Reference yield:

: 86921-46-2
2,4-dimethyl-1-<2-<4-(phenylmethoxy)phenyl>ethyl>-1H-imidazole

: 2-[(Z)-Acetylimino]-N-[2-(4-benzyloxy-phenyl)-ethyl]-propionamide

Guidance literature:: With oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; hematoporphyrin; In tetrahydrofuran; at 23 ℃; for 3.25h; Irradiation;
DOI:10.1021/ja00314a053

Reference yield:

: 86921-46-2
2,4-dimethyl-1-<2-<4-(phenylmethoxy)phenyl>ethyl>-1H-imidazole

: 88336-78-1
2-(acetylamino)-N-<2-<4-(phenylmethoxy)phenyl>ethyl>propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: DBU, hematoporphyrin, oxygen / tetrahydrofuran / 3.25 h / 23 °C / Irradiation

2: KH, tert-butyl alcohol / tetrahydrofuran / Ambient temperature

3: H₂ / (Rh(NBD)Cl)2, (R,R)-DIPAMP / methanol / 760 Torr

With hydrogen; oxygen; potassium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; hematoporphyrin; tert-butyl alcohol; di-μ-chlorobis(norbornadiene)dirhodium(I); (R_P,R_P)-1,2-bis[(o-anisyl)(phenyl)phosphino]ethane; In tetrahydrofuran; methanol;
DOI:10.1021/ja00314a053