Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-

Base Information

Chemical Name:Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-
CAS No.:103595-57-9
Molecular Formula:C₁₉H₂₅NO₅S
Molecular Weight:379.477
Hs Code.:
DSSTox Substance ID:DTXSID10145936
Wikidata:Q83010649

Synonyms:103595-57-9;Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-;BRN 5632306;N-Methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)benzenemethanamine;DTXSID10145936

Suppliers and Price of Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-

Chemical Property:

Vapor Pressure:3.49E-11mmHg at 25°C
Boiling Point:526.7°Cat760mmHg
Flash Point:272.3°C
Density:1.183g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:9
Exact Mass:379.14534407
Heavy Atom Count:26
Complexity:487

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CCS(=O)(=O)C1=CC(=C(C(=C1)OC)OC)OC)CC2=CC=CC=C2

Technology Process of Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)-

There total 8 articles about Benzenemethanamine, N-methyl-N-(2-((2,3,4-trimethoxyphenyl)sulfonyl)ethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 103595-44-4
(Trimethoxy-2,3,4 phenyl)vinylsulfone

: 103-67-3
benzyl-methyl-amine

: 103595-57-9
N-Benzyl N-methyl((trimethoxy-2,3,4 phenyl)sulfonyl)-2 ethylamine

Guidance literature:: In ethanol; for 96h; Ambient temperature;

Reference yield:

: 634-36-6
1,2,3-trimethoxybenzene

: 103595-57-9
N-Benzyl N-methyl((trimethoxy-2,3,4 phenyl)sulfonyl)-2 ethylamine

Guidance literature:: Multi-step reaction with 7 steps

1: 74 percent / cc. H₂SO₄ / 4 h / 25 - 30 °C

2: 79 percent / SOCl₂ / dimethylformamide / 24 h / Ambient temperature

3: 74 percent / Na₂SO₃ / pH 8-9

4: 58 percent / Na₂CO₃ / H₂O / 4 h / Heating; pH neutr.

5: 85 percent / pyridine, SOCl₂ / 3 h / Heating

6: 85 percent / triethylamine / benzene / 24 h / Ambient temperature

7: 83 percent / ethanol / 96 h / Ambient temperature

With pyridine; thionyl chloride; sulfuric acid; sodium carbonate; triethylamine; sodium sulfite; In ethanol; water; N,N-dimethyl-formamide; benzene;

Reference yield:

: 42771-30-2
2,3,4-trimethoxybenzenesulfonyl chloride

: 103595-57-9
N-Benzyl N-methyl((trimethoxy-2,3,4 phenyl)sulfonyl)-2 ethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / Na₂SO₃ / pH 8-9

2: 58 percent / Na₂CO₃ / H₂O / 4 h / Heating; pH neutr.

3: 85 percent / pyridine, SOCl₂ / 3 h / Heating

4: 85 percent / triethylamine / benzene / 24 h / Ambient temperature

5: 83 percent / ethanol / 96 h / Ambient temperature

With pyridine; thionyl chloride; sodium carbonate; triethylamine; sodium sulfite; In ethanol; water; benzene;