ethyl 2,3-dideoxyhexopyranoside

Base Information

Chemical Name:ethyl 2,3-dideoxyhexopyranoside
CAS No.:23339-16-4
Molecular Formula:C8H16 O4
Molecular Weight:176.213
Hs Code.:
Mol file:23339-16-4.mol

Synonyms:D-erythro-Hexopyranoside,ethyl 2,3-dideoxy- (7CI); D-erythro-Hexopyranoside, ethyl 2,3-dideoxy-, a- (8CI); NSC 409806

Suppliers and Price of ethyl 2,3-dideoxyhexopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of ethyl 2,3-dideoxyhexopyranoside

Chemical Property:

Vapor Pressure:5.18E-05mmHg at 25°C
Boiling Point:310.9°C at 760 mmHg
Flash Point:141.9°C
Density:1.15g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 2,3-dideoxyhexopyranoside

There total 14 articles about ethyl 2,3-dideoxyhexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 55735-69-8
ethyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythrohexopyranoside

: 23339-16-4
(2R,3S,6S)-6-ethoxy-2-(hydroxymethyl)tetrahydro-2H-pyran-3-ol

Guidance literature:: With barium dihydroxide;

Reference yield:

: 3323-72-6
ethyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythrohex-2-enopyranoside

: 23339-16-4
(2R,3S,6S)-6-ethoxy-2-(hydroxymethyl)tetrahydro-2H-pyran-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 2.2 g / H₂ / Pd/C / ethanol / 20 °C

2: 1.22 g / MeONa / methanol / 1.5 h / 25 °C

With hydrogen; sodium methylate; palladium on activated charcoal; In methanol; ethanol; 1: Catalytic hydrogenation / 2: Deacetylation;
DOI:10.1007/BF02256842

Reference yield:

: C₅₄H₈₄O₁₁Si₂

: 18107-18-1
diazomethyl-trimethyl-silane

: 23339-16-4
(2R,3S,6S)-6-ethoxy-2-(hydroxymethyl)tetrahydro-2H-pyran-3-ol

Guidance literature:: With boron trifluoride diethyl etherate; In hexane; dichloromethane; at -80 ℃; for 1h; Molecular sieve;
DOI:10.1021/acs.orglett.9b02502