1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)propane-1,3-diol

Base Information

Chemical Name:1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)propane-1,3-diol
CAS No.:22676-00-2
Molecular Formula:C18H22 O6
Molecular Weight:334.369
Hs Code.:
Mol file:22676-00-2.mol

Synonyms:Veratrylalcohol, a-[2-hydroxy-1-(p-methoxyphenoxy)ethyl]-(8CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)propane-1,3-diol

Chemical Property:

Vapor Pressure:4.3E-12mmHg at 25°C
Boiling Point:530.7°Cat760mmHg
Flash Point:274.8°C
Density:1.214g/cm³

Purity/Quality:

Safty Information:

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Technology Process of 1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)propane-1,3-diol

There total 3 articles about 1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)propane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: C₂₀H₂₂O₇

: 22676-00-2
[1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)-1,3-dihydroxypropane]

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1039/c6ra18806k

Reference yield:

: 56606-57-6
ethyl 2-bromo-3-(3,4-dimethoxyphenyl)-3-oxo-propanoate

: 22676-00-2
[1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)-1,3-dihydroxypropane]

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil / 0.25 h

1.2: 9 h / 20 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; water / 24 h / 20 °C

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; water; mineral oil;
DOI:10.1039/c6ra18806k

Reference yield:

: 150-76-5
4-methoxy-phenol

: 22676-00-2
[1-(3,4-dimethoxyphenyl)-2-(4-methoxyphenoxy)-1,3-dihydroxypropane]

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil / 0.25 h

1.2: 9 h / 20 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; water / 24 h / 20 °C

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; water; mineral oil;
DOI:10.1039/c6ra18806k