Benzoic acid, 3,4,5-trimethoxy-, 3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen yl)-2-propenyl]oxy]propyl]amino]propyl ester

Base Information

Chemical Name:Benzoic acid, 3,4,5-trimethoxy-, 3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen yl)-2-propenyl]oxy]propyl]amino]propyl ester
CAS No.:870449-66-4
Molecular Formula:C33H45NO12
Molecular Weight:647.72
Hs Code.:

Benzoic acid, 3,4,5-trimethoxy-,
3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen
yl)-2-propenyl]oxy]propyl]amino]propyl ester

Synonyms:

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Chemical Property of Benzoic acid, 3,4,5-trimethoxy-, 3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen yl)-2-propenyl]oxy]propyl]amino]propyl ester

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Technology Process of Benzoic acid, 3,4,5-trimethoxy-, 3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen yl)-2-propenyl]oxy]propyl]amino]propyl ester

There total 6 articles about Benzoic acid, 3,4,5-trimethoxy-, 3-[[(1,1-dimethylethoxy)carbonyl][3-[[(2E)-1-oxo-3-(3,4,5-trimethoxyphen yl)-2-propenyl]oxy]propyl]amino]propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870449-49-3
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-bromopropyl ester

: 870449-66-4
3,4,5-trimethoxybenzoic acid 3-(N-tert-butoxycarbonyl[3-[trans-3-(3,4,5-trimethoxyphenyl)acryloiloxy]propyl]amino)propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetonitrile / 60 °C

2: 95 percent / Et₃N / tetrahydrofuran / 6 h / 20 °C

3: 180 mg / CHCl₃ / 60 °C

With potassium carbonate; triethylamine; In tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1021/jm050542x

Reference yield:

: 870449-56-2
trans-3-(3,4,5-trimethoxyphenyl)acrylic acid 3-(3-hydroxypropylamino)propyl ester

: 870449-66-4
3,4,5-trimethoxybenzoic acid 3-(N-tert-butoxycarbonyl[3-[trans-3-(3,4,5-trimethoxyphenyl)acryloiloxy]propyl]amino)propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N / tetrahydrofuran / 6 h / 20 °C

2: 180 mg / CHCl₃ / 60 °C

With triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1021/jm050542x

Reference yield:

: 20329-98-0,20329-99-1,90-50-6
(E)-3,4,5-trimethoxy-cinnamic acid

: 870449-66-4
3,4,5-trimethoxybenzoic acid 3-(N-tert-butoxycarbonyl[3-[trans-3-(3,4,5-trimethoxyphenyl)acryloiloxy]propyl]amino)propyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂ / benzene / 60 °C

2: CHCl₃ / 60 °C

3: K₂CO₃ / acetonitrile / 60 °C

4: 95 percent / Et₃N / tetrahydrofuran / 6 h / 20 °C

5: 180 mg / CHCl₃ / 60 °C

With thionyl chloride; potassium carbonate; triethylamine; In tetrahydrofuran; chloroform; acetonitrile; benzene;
DOI:10.1021/jm050542x