tert-Butyl 4-carbamoylbenzylcarbamate

Base Information

Chemical Name:tert-Butyl 4-carbamoylbenzylcarbamate
CAS No.:871721-44-7
Molecular Formula:C13H18N2O3
Molecular Weight:250.298
Hs Code.:2924299090
Mol file:871721-44-7.mol

Synonyms:tert-Butyl 4-carbamoylbenzylcarbamate;

Suppliers and Price of tert-Butyl 4-carbamoylbenzylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl4-carbamoylbenzylcarbamate 95+%
1g
$ 339.00

Chemenu
tert-butyl(4-carbamoylbenzyl)carbamate 95%
1g
$ 320.00

Alichem
tert-Butyl4-carbamoylbenzylcarbamate
1g
$ 270.48

Activate Scientific
tert-Butyl4-carbamoylbenzylcarbamate 95%
1 g
$ 245.00

Abosyn
tert-butyl4-carbamoylbenzylcarbamate 95%-98%
1g
$ 667.00

Total 6 raw suppliers

Chemical Property of tert-Butyl 4-carbamoylbenzylcarbamate

Chemical Property:

PSA：84.91000
LogP:2.71490
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl4-carbamoylbenzylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-Butyl 4-carbamoylbenzylcarbamate

There total 4 articles about tert-Butyl 4-carbamoylbenzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 369-53-9
4-(aminomethyl)benzamide

: 871721-44-7
tert-butyl 4-carbamoylbenzylcarbamate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield: 85.0%

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 871721-44-7
tert-butyl 4-carbamoylbenzylcarbamate

Guidance literature:: 4-(tert-Butoxycarbonylaminomethyl)benzoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

With ammonia; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1021/ja108212v

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 871721-44-7
tert-butyl 4-carbamoylbenzylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 15 h / 4 - 20 °C / Inert atmosphere

1.2: pH 2 / Inert atmosphere

2.1: ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide; acetonitrile / 22 h / 4 - 20 °C / Inert atmosphere

With ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja209924v