6-Octen-4-one, 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2,6-dimethyl-8-[(1S)-1-methyl-2-[ (phenylmethoxy)methyl]-2-cyclopenten-1-yl]-, (2R,6Z)-

Base Information

Chemical Name:6-Octen-4-one, 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2,6-dimethyl-8-[(1S)-1-methyl-2-[ (phenylmethoxy)methyl]-2-cyclopenten-1-yl]-, (2R,6Z)-
CAS No.:871823-44-8
Molecular Formula:C₃₀H₄₈O₃Si
Molecular Weight:484.795
Hs Code.:

Synonyms:

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Chemical Property of 6-Octen-4-one, 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2,6-dimethyl-8-[(1S)-1-methyl-2-[ (phenylmethoxy)methyl]-2-cyclopenten-1-yl]-, (2R,6Z)-

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Technology Process of 6-Octen-4-one, 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2,6-dimethyl-8-[(1S)-1-methyl-2-[ (phenylmethoxy)methyl]-2-cyclopenten-1-yl]-, (2R,6Z)-

There total 23 articles about 6-Octen-4-one, 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2,6-dimethyl-8-[(1S)-1-methyl-2-[ (phenylmethoxy)methyl]-2-cyclopenten-1-yl]-, (2R,6Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 5-(tert-butyl-dimethyl-silanyloxy)-2-(2-ethoxy-ethoxy)-4-methyl-pentanenitrile

: 871823-53-9
[(S)-5-((Z)-4-Chloro-3-methyl-but-2-enyl)-5-methyl-cyclopent-1-enylmethoxymethyl]-benzene

: 871823-44-8
(Z)-(R)-8-((S)-2-Benzyloxymethyl-1-methyl-cyclopent-2-enyl)-1-(tert-butyl-dimethyl-silanyloxy)-2,6-dimethyl-oct-6-en-4-one

Guidance literature:: With sodium hexamethyldisilazane;
DOI:10.1016/j.tetlet.2005.11.021

Reference yield:

: (R)-2-Hydroxy-4-methyl-5-(tetrahydro-pyran-2-yloxy)-pentanenitrile

: 871823-44-8
(Z)-(R)-8-((S)-2-Benzyloxymethyl-1-methyl-cyclopent-2-enyl)-1-(tert-butyl-dimethyl-silanyloxy)-2,6-dimethyl-oct-6-en-4-one

Guidance literature:: Multi-step reaction with 5 steps

1: PPTS

2: 49 percent / NaHDMS

3: 81 percent / CH₃OH / PPTS

4: imidazole

5: NaOH / H₂O

With 1H-imidazole; methanol; sodium hydroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; In water;
DOI:10.1016/j.tetlet.2005.09.106

Reference yield:

: 170572-77-7
(2'RS,3R)-3-methyl-4-(2-tetrahydropyranyloxy)butanal

: 871823-44-8
(Z)-(R)-8-((S)-2-Benzyloxymethyl-1-methyl-cyclopent-2-enyl)-1-(tert-butyl-dimethyl-silanyloxy)-2,6-dimethyl-oct-6-en-4-one

Guidance literature:: Multi-step reaction with 7 steps

1: 18-crown-6

2: H₂O

3: PPTS

4: 49 percent / NaHDMS

5: 81 percent / CH₃OH / PPTS

6: imidazole

7: NaOH / H₂O

With 1H-imidazole; methanol; sodium hydroxide; water; sodium hexamethyldisilazane; 18-crown-6 ether; pyridinium p-toluenesulfonate; In water;
DOI:10.1016/j.tetlet.2005.09.106