1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)-

Base Information

Chemical Name:1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)-
CAS No.:872624-62-9
Molecular Formula:C17H23F3N2O2
Molecular Weight:344.377
Hs Code.:2933990090
Mol file:872624-62-9.mol

Synonyms:

Suppliers and Price of 1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(S)-tert-Butyl5-amino-7-methyl-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine-1-carboxylate 95+%
1g
$ 987.00

Chemenu
tert-butyl(S)-5-amino-7-methyl-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine-1-carboxylate 95%
1g
$ 931.00

American Custom Chemicals Corporation
(S)-TERT-BUTYL 5-AMINO-7-METHYL-8-(TRIFLUOROMETHYL)-2,3,4,5-TETRAHYDRO-1H-BENZO[B]AZEPINE-1-CARBOXYLATE 95.00%
1G
$ 8354.85

American Custom Chemicals Corporation
(S)-TERT-BUTYL 5-AMINO-7-METHYL-8-(TRIFLUOROMETHYL)-2,3,4,5-TETRAHYDRO-1H-BENZO[B]AZEPINE-1-CARBOXYLATE 95.00%
5MG
$ 502.11

Alichem
(S)-tert-Butyl5-amino-7-methyl-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine-1-carboxylate
1g
$ 824.00

Total 3 raw suppliers

Chemical Property of 1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)-

Chemical Property:

PSA：55.56000
LogP:5.31420
Storage Temp.:2-8°C

Purity/Quality:

≥99% ^*data from raw suppliers

(S)-tert-Butyl5-amino-7-methyl-8-(trifluoromethyl)-2,3,4,5-tetrahydro-1H-benzo[b]azepine-1-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)-

There total 1 articles about 1H-1-Benzazepine-1-carboxylic acid, 5-aMino-2,3,4,5-tetrahydro-7-Methyl-8-(trifluoroMethyl)-, 1,1-diMethylethyl ester, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 872624-61-8
(S)-tert-butyl 5-azido-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate

: 872624-62-9
(S)-tert-butyl 5-amino-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In methanol; at 20 ℃; for 12h; under 1034.32 Torr;

Reference yield: 98.0%

: 872624-62-9
(S)-tert-butyl 5-amino-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate

: 401-95-6
3,5-Bis(trifluoromethyl)benzaldehyde

: 872624-63-0
(S)-tert-butyl 5-(3,5-bistrifluoromethylbenzylamino)-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate

Guidance literature:: (S)-tert-butyl 5-amino-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate; 3,5-Bis(trifluoromethyl)benzaldehyde; In methanol; at 20 ℃; for 2h;

With methanol; sodium tetrahydroborate; for 2h;

Reference yield: 98.0%

: 872624-62-9
(S)-tert-butyl 5-amino-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate

: 188815-30-7
3-fluoro-5-(trifluoromethyl)benzaldehyde

: 872626-73-8
(S)-5-(3-fluoro-5-trifluoromethyl-benzylamino)-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydro-benzo[6]azepine-1-carboxylic acid tert-butyl ester

Guidance literature:: (S)-tert-butyl 5-amino-7-methyl-8-trifluoromethyl-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylate; 3-fluoro-5-(trifluoromethyl)benzaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 20h;

With water; sodium hydrogencarbonate; In 1,2-dichloro-ethane;