3-Fluoro-3-phenyl-3H-diazirine

Base Information

Chemical Name:3-Fluoro-3-phenyl-3H-diazirine
CAS No.:87282-19-7
Molecular Formula:C7H5FN2
Molecular Weight:136.129
Hs Code.:
DSSTox Substance ID:DTXSID50518827
Nikkaji Number:J1.899.088A

Synonyms:3-Fluoro-3-phenyl-3H-diazirine;87282-19-7;3-Fluoro-3-phenyl-3H-diazirene;DTXSID50518827

Suppliers and Price of 3-Fluoro-3-phenyl-3H-diazirine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Fluoro-3-phenyl-3H-diazirine

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:136.04367633
Heavy Atom Count:10
Complexity:155

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2(N=N2)F

Technology Process of 3-Fluoro-3-phenyl-3H-diazirine

There total 3 articles about 3-Fluoro-3-phenyl-3H-diazirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4460-46-2
3-chloro-3-phenyl-3H-diazirine

: 87282-19-7
3-fluoro-3-phenyldiazirine

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; at 25 ℃; for 16h;
DOI:10.1021/ja00359a038

Reference yield: 65.0%

: 4222-25-7
3-bromo-3-phenyl-3H-diazirine

: 87282-19-7
3-fluoro-3-phenyldiazirine

Guidance literature:: With tetrabutyl ammonium fluoride; at 25 ℃; for 4h;
DOI:10.1021/ja00359a038

Reference yield:

: 1670-14-0
benzamidine monohydrochloride

: 87282-19-7
3-fluoro-3-phenyldiazirine

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / NaOBr, LiBr / dimethylsulfoxide / 1 h

2: 65 percent / molten tetrabutylammonium fluoride / 4 h / 25 °C

With sodium hypobromide; tetrabutyl ammonium fluoride; lithium bromide; In dimethyl sulfoxide;
DOI:10.1021/ja00295a029