Tetrahydrothiopyran-4-one oxiMe

Base Information

• Chemical Name: Tetrahydrothiopyran-4-one oxiMe
• CAS No.: 6309-59-7
• Molecular Formula: C5H9 N O S
• Molecular Weight: 131.1961
• Hs Code.: 2934999090
• Mol file: 6309-59-7.mol

Synonyms:NSC41600; Tetrahydro-4H-thiopyran-4-one oxime;Tetrahydrothiopyran-4-one oxime

Chemical Property of Tetrahydrothiopyran-4-one oxiMe

Chemical Property:

• Vapor Pressure: 0.00107mmHg at 25°C
• Boiling Point: 279.4°Cat760mmHg
• Flash Point: 122.8°C
• PSA: 57.89000
• Density: 1.3g/cm³
• LogP: 1.34360
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

Tetrahydrothiopyran-4-one oxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tetrahydrothiopyran-4-one oxiMe

There total 3 articles about Tetrahydrothiopyran-4-one oxiMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Tetrahydrothiopyran-4-one (1072-72-6) → tetrahydro-4H-thiopyran-4-one oxime (6309-59-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; for 6h; Heating / reflux;

Reference yield:

Tetrahydrothiopyran-4-one (1072-72-6) → tetrahydro-4H-thiopyran-4-one oxime (6309-59-7) + thianone oxime

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate trihydrate; In ethanol;

Reference yield:

→ tetrahydro-4H-thiopyran-4-one oxime (6309-59-7)

Guidance literature:

Thian-4-on, Hydroxylamin;

DOI:10.1002/hlca.19740570832

upstream raw materials:

Tetrahydrothiopyran-4-one

Downstream raw materials:

4-tetrahydrothiopyranylamine

Thian-4-on-oxim-p-toluolsulfonat

4-(5-chloro-2-cyclopropyl-1H-pyrrolo[2,3-b]pyridin-4-yl)-N-(1,1-dioxotetrahydro-2H-thiopyran-4-yl)benzenesulfonamide

4-(2-cyclopropyl-5-fluoro-1H-pyrrolo[2,3-b]pyridin-4-yl)-N-(1,1-dioxidotetrahydro-2H-thiopyran-4-yl)benzenesulfonamide

Refernces

• 1、 -. "SUBSTITUTED PHENYLOXAZOLIDINONES FOR ANTIMICROBIAL THERAPY". Page/Page column 28; 29. . Retrieved 2017/02/09.
• 2、 -. "AZEPANE DERIVATIVES AND METHODS OF TREATING HEPATITIS B INFECTIONS". Paragraph 0774. . Retrieved 2015/09/22.