2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate

Base Information

• Chemical Name: 2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate
• CAS No.: 19461-93-9
• Molecular Formula: C14H21ClN2O4S
• Molecular Weight: 348.8455
• Mol file: 19461-93-9.mol

Synonyms:2-p-Dimethylaminophenyl-3-methyl-4-ethyl-2-thiazolinium perchlorate;2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate;19461-93-9;C14H21N2S.ClO4;C14-H21-N2-S.Cl-O4;LS-151912

Chemical Property of 2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 348.0910560
• Heavy Atom Count: 22
• Complexity: 386

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1CSC(=[N+]1C)C2=CC=C(C=C2)N(C)C.[O-]Cl(=O)(=O)=O

Technology Process of 2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate

There total 2 articles about 2-Thiazolinium, 2-(p-(dimethylamino)phenyl)-4-ethyl-3-methyl-, perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(dimethylamino)-N-methylbenzamide (21176-94-3) → 2-(4-dimethylamino-phenyl)-4-ethyl-3-methyl-4,5-dihydro-thiazolium; perchlorate (19461-93-9)

Guidance literature:

Multi-step reaction with 2 steps

1: P₂S₅, Py

2: (i) ethoxyethanol, (ii) NaOAc, (iii) aq. NaClO₄

With pyridine; tetraphosphorus decasulfide;

DOI:10.1021/jm00312a021

Reference yield:

1,4-dibromo-butane (110-52-1) + 4-dimethylamino-N-methyl-thiobenzamide (21176-93-2) → 2-(4-dimethylamino-phenyl)-4-ethyl-3-methyl-4,5-dihydro-thiazolium; perchlorate (19461-93-9)

Guidance literature:

Multistep reaction; (i) ethoxyethanol, (ii) NaOAc, (iii) aq. NaClO₄;

DOI:10.1021/jm00312a021

upstream raw materials:

1,4-dibromo-butane

4-dimethylamino-N-methyl-thiobenzamide

4-(dimethylamino)-N-methylbenzamide