Chromium,amminepentacarbonyl-, (OC-6-22)-

Base Information

Chemical Name:Chromium,amminepentacarbonyl-, (OC-6-22)-
CAS No.:15228-27-0
Molecular Formula:C5H3 Cr N O5
Molecular Weight:209.079
Hs Code.:

Synonyms:Chromium,amminepentacarbonyl- (7CI,8CI); Amminepentacarbonylchromium

Suppliers and Price of Chromium,amminepentacarbonyl-, (OC-6-22)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Chromium,amminepentacarbonyl-, (OC-6-22)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Chromium,amminepentacarbonyl-, (OC-6-22)-

There total 2 articles about Chromium,amminepentacarbonyl-, (OC-6-22)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 41371-94-2,14974-11-9,96647-88-0
tris(ammonia)chromium tricarbonyl

: 5350-57-2
benzophenone hydrazone

: 15228-27-0
pentacarbonyl(ammonia)chromium

: 170955-30-3
(C₆H₅CNNH₂C₆H₅)Cr(CO)3

: (C₆H₅)2CNNH₂*Cr*5CO=(C₆H₅)2CNNH₂*Cr(CO)5

Guidance literature:: In 1,4-dioxane; reflux (1 h, Ar-atmosphere), cooling; ppt. filtration off (silica gel), solvent removing, residue dissoln. in benzene, chromy. (silica gel/hexane-benzene); elem. anal.;
DOI:10.1007/BF00698519

Reference yield: 13.5%

: 117696-62-5
C₄H₄B(C₆H₅)(NH₃)

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 15228-27-0
pentacarbonyl(ammonia)chromium

: (CO)4Cr(C₄H₄BC₆H₅)Cr(CO)3

: tetracarbonyl{η5-(1-phenylborole)}chromium

Guidance literature:: With THF; In tetrahydrofuran; Irradiation (UV/VIS); soln. of Cr(CO)5(THF) in THF prepd. from Cr(CO)6 by exhaustive irrdn. with 150 W high pressure Hg lamp (TQ 150, Original Hanau) under N2, soln. of C4H4B(Ph)(NH3) in THF added, kept at 65°C for 5 h; evapd.(vac.), extd.(pentane), filtered, concd., cooled(-30°C), chromd. (Al2O3/7% H2O(water-cooled,light protected column); pentane, pentane/ether(4/1)), concd.(vac.), dried(1E-5 bar/-78°C), sublimed(1E-5 bar), crystd.(hexane); elem. anal.;
DOI:10.1016/0022-328X(87)87155-3