1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid

Base Information

Chemical Name:1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid
CAS No.:23673-45-2
Molecular Formula:C₁₄H₁₆O₅
Molecular Weight:264.278
Hs Code.:
NSC Number:165195
DSSTox Substance ID:DTXSID10946485
Mol file:23673-45-2.mol

Synonyms:23673-45-2;1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid;NSC165195;NSC 165195;1-hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexane-1-carboxylic acid;DTXSID10946485;NSC-165195;1-hydroxy-2-(4-methoxyphenyl)-5-oxo-cyclohexanecarboxylic acid

Suppliers and Price of 1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid

Chemical Property:

Vapor Pressure:9.96E-11mmHg at 25°C
Boiling Point:497.8°C at 760 mmHg
Flash Point:190.8°C
Density:1.329g/cm³
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:264.09977361
Heavy Atom Count:19
Complexity:359

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2CCC(=O)CC2(C(=O)O)O

Technology Process of 1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid

There total 1 articles about 1-Hydroxy-2-(4-methoxyphenyl)-5-oxocyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23673-45-2
1-Hydroxy-5-oxo-2-(p-methoxy-phenyl)-cyclohexancarbonsaeure

Guidance literature:: p-Methoxy-phenyl-brenztraubensaeure, Methylvinylketon / wss.methanol.NaOH;
DOI:10.1016/S0040-4039(01)88151-X

Reference yield:

: 23673-45-2
1-Hydroxy-5-oxo-2-(p-methoxy-phenyl)-cyclohexancarbonsaeure

: 23668-28-2,138403-95-9
cis-6-(4'-methoxyphenyl)-3-oxocyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 180 - 190 °C

2: H₂ / Pd-C / ethanol

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00823a010

Reference yield:

: 23673-45-2
1-Hydroxy-5-oxo-2-(p-methoxy-phenyl)-cyclohexancarbonsaeure

: 31730-01-5
cis-2-(p-Methoxyphenyl)-5-oxo-1-cyclohexancarbonsaeuremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 180 - 190 °C

2: H₂ / Pd-C / ethanol

3: diethyl ether

With hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jo00823a010