beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate

Base Information

• Chemical Name: beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate
• CAS No.: 84582-23-0
• Molecular Formula: C24H36O10
• Molecular Weight: 484.544
• Mol file: 84582-23-0.mol

Synonyms:(+-)-alpha-Terpineol-2,3,4,6-tetra-O-acetyl-beta-D-glucopyranoside;beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate;84582-23-0;C26-H36-O10;LS-71565

Chemical Property of beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate

Chemical Property:

• Vapor Pressure: 1.78E-13mmHg at 25°C
• Boiling Point: 530.6°Cat760mmHg
• Flash Point: 166.6°C
• PSA: 134.66000
• Density: 1.22g/cm³
• LogP: 2.20460
• XLogP3: 2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 11
• Exact Mass: 484.23084734
• Heavy Atom Count: 34
• Complexity: 832

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CCC(CC1)C(C)(C)C2(C(C(C(C(O2)CO)OC(=O)C)OC(=O)C)OC(=O)C)OC(=O)C
• Isomeric SMILES: CC1=CCC(CC1)C(C)(C)[C@@]2([C@@H]([C@H]([C@@H]([C@H](O2)CO)OC(=O)C)OC(=O)C)OC(=O)C)OC(=O)C

Technology Process of beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate

There total 2 articles about beta-D-Glucopyranoside, 1-methyl-1-(4-methyl-3-cyclohexen-1-yl)ethyl, tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

terpineol (98-55-5,2438-12-2) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → (+/-)-α-terpineol-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (84582-23-0)

Guidance literature:

With mercury(II) cyanide; In benzene; at 130 ℃; for 0.5h;

DOI:10.1248/cpb.33.1669

Reference yield:

terpineol (98-55-5,2438-12-2) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide → (+/-)-α-terpineol-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (84582-23-0)

Guidance literature:

With silver(l) oxide; In diethyl ether; for 288h; Ambient temperature;

DOI:10.1016/0031-9422(82)83034-3

Reference yield:

(+/-)-α-terpineol-2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside (84582-23-0) → (+/-)-α-terpineol-β-D-O-glucopyranoside (39015-85-5)

Guidance literature:

With sodium methylate; In methanol; for 0.25h; Ambient temperature;

DOI:10.1248/cpb.33.1669

upstream raw materials:

terpineol

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

(+/-)-α-terpineol-β-D-O-glucopyranoside

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