Silane, [(3,4-dihydro-2H-pyran-2-yl)methoxy](1,1-dimethylethyl)diphenyl-

Base Information

Chemical Name:Silane, [(3,4-dihydro-2H-pyran-2-yl)methoxy](1,1-dimethylethyl)diphenyl-
CAS No.:873309-58-1
Molecular Formula:C22H28O2Si
Molecular Weight:352.549
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, [(3,4-dihydro-2H-pyran-2-yl)methoxy](1,1-dimethylethyl)diphenyl-

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Technology Process of Silane, [(3,4-dihydro-2H-pyran-2-yl)methoxy](1,1-dimethylethyl)diphenyl-

There total 2 articles about Silane, [(3,4-dihydro-2H-pyran-2-yl)methoxy](1,1-dimethylethyl)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3749-36-8
2-hydroxymethyl-3,4-dihydro-2H-pyran

: 58479-61-1
tert-butylchlorodiphenylsilane

: 873309-58-1
tert-butyl ((3,4-dihydro-2H-pyran-2-yl)methoxy)diphenylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2006.01.051

Reference yield:

: 100-73-2
acrolein dimer

: 873309-58-1
tert-butyl ((3,4-dihydro-2H-pyran-2-yl)methoxy)diphenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaBH₄ / ethanol / 5 h / -78 - 20 °C

2: 100 percent / imidazole / dimethylformamide / 2 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.01.051

Reference yield: 92.4%

: 873309-58-1
tert-butyl ((3,4-dihydro-2H-pyran-2-yl)methoxy)diphenylsilane

: trans-6-(tert-butyl-diphenyl-silanyloxymethyl)-tetrahydro-pyran-3-ol

Guidance literature:: tert-butyl-(3,4-dihydro-2H-pyran-2-yl-methoxy)-diphenylsilane; With borane; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 55 ℃; for 1h;
DOI:10.1016/j.bmc.2006.01.051