L-Phenylalanine, 2,3,4,5-tetrafluoro-

Base Information

Chemical Name:L-Phenylalanine, 2,3,4,5-tetrafluoro-
CAS No.:873429-68-6
Molecular Formula:C9H7F4NO2
Molecular Weight:237.154
Hs Code.:

Synonyms:

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Chemical Property of L-Phenylalanine, 2,3,4,5-tetrafluoro-

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Technology Process of L-Phenylalanine, 2,3,4,5-tetrafluoro-

There total 8 articles about L-Phenylalanine, 2,3,4,5-tetrafluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1093786-41-4
(S)-2-amino-3-(2,3,4,5-tetrafluorophenyl)propionic acid N-methylamide

: 873429-68-6
(S)-2-amino-3-(2,3,4,5-tetrafluorophenyl)propionic acid

Guidance literature:: (S)-2-amino-3-(2,3,4,5-tetrafluorophenyl)propionic acid N-methylamide; With potassium hydroxide; In water; for 2.5h; Reflux;

With hydrogenchloride; In water;

Reference yield: 92.0%

: C₁₁H₉F₄NO₃

: 873429-68-6
(S)-2-amino-3-(2,3,4,5-tetrafluorophenyl)propionic acid

Guidance literature:: With Aspergillus genus acylase; acetic acid; sodium hydroxide; at 38 ℃; Enzymatic reaction;
DOI:10.1016/j.bmc.2021.116498

Reference yield:

: 53001-71-1
2,3,4,5-tetrafluorobenzyl bromide

: 873429-68-6
(S)-2-amino-3-(2,3,4,5-tetrafluorophenyl)propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium / ethanol / 2 h / 70 °C

2: sodium hydroxide; methanol / 3 h / 40 °C

3: para-xylene / Reflux

4: acetic acid; sodium hydroxide; Aspergillus genus acylase / 48 h / 38 °C / Enzymatic reaction

5: acetic acid; sodium hydroxide; Aspergillus genus acylase / 38 °C / Enzymatic reaction

With methanol; Aspergillus genus acylase; sodium; acetic acid; sodium hydroxide; In ethanol; para-xylene;
DOI:10.1016/j.bmc.2021.116498