4-(METHYLNITROSOAMINO)-1-(3-PYRIDYL)-1-BUTANONE

Base Information

• Chemical Name: 4-(METHYLNITROSOAMINO)-1-(3-PYRIDYL)-1-BUTANONE
• CAS No.: 64091-50-5
• Molecular Formula: C₂₉H₃₇N₃O₂
• Molecular Weight: 459.632
• Mol file: 64091-50-5.mol

Synonyms:Indolo[2,3-a]quinolizine,17-norcorynan deriv.; Pseudotubulosine d

Chemical Property of 4-(METHYLNITROSOAMINO)-1-(3-PYRIDYL)-1-BUTANONE

Chemical Property:

• PSA: 62.63000
• LogP: 1.65770

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(METHYLNITROSOAMINO)-1-(3-PYRIDYL)-1-BUTANONE

There total 23 articles about 4-(METHYLNITROSOAMINO)-1-(3-PYRIDYL)-1-BUTANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 1-((2S,3S,12bS)-3-Ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl)-1,2,3,4-tetrahydro-isoquinoline-6,7-diol → 2-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-47-0,64091-48-1,64091-49-2,64091-50-5,64129-83-5) + 2-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-47-0,64091-48-1,64091-49-2,64091-50-5,64129-83-5)

Guidance literature:

In diethyl ether; ethanol; at 4 ℃; for 48h;

DOI:10.1002/hlca.19800630525

Reference yield: 17.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 1-((2S,3S,12bS)-3-Ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-ylmethyl)-1,2,3,4-tetrahydro-isoquinoline-6,7-diol → 2-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-47-0,64091-48-1,64091-49-2,64091-50-5,64129-83-5) + 2-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-47-0,64091-48-1,64091-49-2,64091-50-5,64129-83-5)

Guidance literature:

In diethyl ether; ethanol; at 4 ℃; for 48h;

DOI:10.1002/hlca.19800630525

Reference yield:

(2R,3S,12bS)-2-(6,7-Dimethoxy-3,4-dihydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-55-0) → 2-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine (64091-47-0,64091-48-1,64091-49-2,64091-50-5,64129-83-5)

Guidance literature:

With potassium borohydride; In methanol; for 24h; Ambient temperature;

DOI:10.1002/hlca.19800630525

upstream raw materials:

(2R,3S,12bS)-2-(6,7-Dimethoxy-3,4-dihydro-isoquinolin-1-ylmethyl)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

2-(3,4-dimethoxyphenyl)-ethylamine

N-[2-(3,4-Dimethoxy-phenyl)-ethyl]-2-((2R,3S,12bS)-3-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-2-yl)-acetamide

(2R,3R,12bS)-3-ethyl-2-(methoxycarbonylmethyl)-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizine

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