n-(4-Amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide

Base Information

• Chemical Name: n-(4-Amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide
• CAS No.: 6336-83-0
• Molecular Formula: C17H14N2O3
• Molecular Weight: 294.3047
• NSC Number: 39893
• DSSTox Substance ID: DTXSID30284932
• Wikidata: Q82020120
• Mol file: 6336-83-0.mol

Synonyms:6336-83-0;n-(4-amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide;NSC39893;DTXSID30284932;NSC-39893

Chemical Property of n-(4-Amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide

Chemical Property:

• Vapor Pressure: 1.01E-12mmHg at 25°C
• Boiling Point: 563.5°Cat760mmHg
• Flash Point: 294.6°C
• Density: 1.381g/cm³
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 1
• Exact Mass: 294.10044231
• Heavy Atom Count: 22
• Complexity: 504

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)N(C)C1=C2C(=C(C=C1)N)C(=O)C3=CC=CC=C3C2=O

Technology Process of n-(4-Amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide

There total 2 articles about n-(4-Amino-9,10-dioxo-9,10-dihydroanthracen-1-yl)-n-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-acetylamino-4-N-acetylmethylaminoanthraquinone (77817-45-9) → 1-amino-4-N-acetylmethylaminoanthraquinone (6336-83-0)

Guidance literature:

With sodium hydroxide; In ethanol; for 0.5h; Ambient temperature;

Reference yield:

1-amino-4-(methylamino)anthraquinone (1220-94-6) → 1-amino-4-N-acetylmethylaminoanthraquinone (6336-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄ / Ambient temperature

2: 97 percent / NaOH / ethanol / 0.5 h / Ambient temperature

With sodium hydroxide; sulfuric acid; In ethanol;

Reference yield:

1-amino-4-N-acetylmethylaminoanthraquinone (6336-83-0) → 6-amino-N-methylanthrapyridone (14642-72-9)

Guidance literature:

With sodium hydroxide;

upstream raw materials:

1-acetylamino-4-N-acetylmethylaminoanthraquinone

1-amino-4-(methylamino)anthraquinone

Downstream raw materials:

6-amino-N-methylanthrapyridone