Technology Process of Diospyrol
There total 12 articles about Diospyrol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aq. KOH / methanol
2: K2CO3
3: LiAlH4
4: H2, HClO4 / Pd-C
5: BCl3
With
potassium hydroxide; lithium aluminium tetrahydride; perchloric acid; hydrogen; boron trichloride; potassium carbonate;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 74 percent / tetrahydrofuran / -78 deg C to room temp., overnight
2: 30 percent aq. NaOH / dioxane; methanol / Heating
3: TsOH / methanol / Heating
4: DDQ / benzene / Ambient temperature
5: 85 percent / BCl3 / CH2Cl2 / -60 deg C to room temp.
With
sodium hydroxide; boron trichloride; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; benzene;
DOI:10.1016/S0040-4039(01)80678-X
