Ethanol, 2-[[(2Z)-3-phenyl-2-propenyl]oxy]-

Base Information

Chemical Name:Ethanol, 2-[[(2Z)-3-phenyl-2-propenyl]oxy]-
CAS No.:873692-42-3
Molecular Formula:C11H14O2
Molecular Weight:178.231
Hs Code.:

Synonyms:

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Chemical Property of Ethanol, 2-[[(2Z)-3-phenyl-2-propenyl]oxy]-

Chemical Property:

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Technology Process of Ethanol, 2-[[(2Z)-3-phenyl-2-propenyl]oxy]-

There total 1 articles about Ethanol, 2-[[(2Z)-3-phenyl-2-propenyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4510-34-3
(Z)-cinnamyl alcohol

: 873692-42-3
(Z)-2-(3-phenylprop-2-enyloxy)ethan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / benzene / Heating

2: 603 mg / LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether; benzene;
DOI:10.1021/jo051652e

Reference yield:

: 873692-42-3
(Z)-2-(3-phenylprop-2-enyloxy)ethan-1-ol

: (Z)-(3-phenylprop-2-enyloxy)acetaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1021/jo051652e

Reference yield:

: 873692-42-3
(Z)-2-(3-phenylprop-2-enyloxy)ethan-1-ol

: 873692-44-5
(Z)-(3-phenylprop-2-enyloxy)acetaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: DMSO; oxalyl chloride; triethylamine / CH₂Cl₂ / 0 °C

2: 640 mg / NH₂OH*HCl; NaHCO₃ / ethanol; H₂O / 20 °C

With oxalyl dichloride; hydroxylamine hydrochloride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; water; 1: Swern oxidation;
DOI:10.1021/jo051652e