4'-O-Methylnorbelladine

Base Information Edit

Chemical Name:4'-O-Methylnorbelladine
CAS No.:4579-60-6
Molecular Formula:C16H19NO3
Molecular Weight:273.332
Hs Code.:2922509090
NSC Number:77594
DSSTox Substance ID:DTXSID50291729
Nikkaji Number:J1.010.314B
Wikidata:Q27149709
ChEMBL ID:CHEMBL4471934
Mol file:4579-60-6.mol

Synonyms:4579-60-6;4'-O-Methylnorbelladine;N-(p-Hydroxyphenethyl)-N-(3-hydroxy-4-methoxy)benzylamine;5-[[2-(4-hydroxyphenyl)ethylamino]methyl]-2-methoxyphenol;5-({[2-(4-Hydroxyphenyl)ethyl]amino}methyl)-2-methoxyphenol;5-(([2-(4-Hydroxyphenyl)ethyl]amino)methyl)-2-methoxyphenol;INETERMEDIATEOFGALANTHAMINE1;NSC77594;N-isovanillyltyramine;Probes1_000056;Probes2_000396;SCHEMBL1719403;CHEMBL4471934;CHEBI:80667;DTXSID50291729;SDLILULALIDNSO-UHFFFAOYSA-N;MFCD01444586;NSC-77594;AKOS000280536;CS-0452730;FT-0669936;F87974;Q27149709;5-(((4-Hydroxyphenethyl)amino)methyl)-2-methoxyphenol;2-Benzenol,1-methoxy-4-[[[2-(4-hydroxyphenyl)ethyl]amino]methyl]-;5-(([2-(4-Hydroxyphenyl)ethyl]amino)methyl)-2-methoxyphenol #

Suppliers and Price of 4'-O-Methylnorbelladine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-(p-Hydroxyphenethyl)-N-(3-hydroxy-4-methoxy)benzylamine
2g
$ 545.00

Medical Isotopes, Inc.
N-(p-Hydroxyphenethyl)-N-(3-hydroxy-4-methoxy)benzylamine
2.5 g
$ 2000.00

American Custom Chemicals Corporation
N-(P-HYDROXYPHENETHYL)-N-(3-HYDROXY-4-METHOXY)BENZYLAMINE 95.00%
5G
$ 1905.75

American Custom Chemicals Corporation
N-(P-HYDROXYPHENETHYL)-N-(3-HYDROXY-4-METHOXY)BENZYLAMINE 95.00%
500MG
$ 721.88

Total 12 raw suppliers

Chemical Property of 4'-O-Methylnorbelladine Edit

Chemical Property:

Vapor Pressure:1.79E-17mmHg at 25°C
Melting Point:183-185oC
Boiling Point:471.8°Cat760mmHg
Flash Point:239.1°C
PSA：61.72000
Density:1.192g/cm³
LogP:2.82960
Storage Temp.:Refrigerator
Solubility.:DMSO (Slightly), Methanol (Slightly, Heated)
XLogP3:2.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:273.13649347
Heavy Atom Count:20
Complexity:266

Purity/Quality:

99%min ^*data from raw suppliers

N-(p-Hydroxyphenethyl)-N-(3-hydroxy-4-methoxy)benzylamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CNCCC2=CC=C(C=C2)O)O
Uses N-(p-Hydroxyphenethyl)-N-(3-hydroxy-4-methoxy)benzylamine (cas# 4579-60-6) is a compound useful in organic synthesis.

Technology Process of 4'-O-Methylnorbelladine

There total 8 articles about 4'-O-Methylnorbelladine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.1%

: 621-59-0
isovanillin

: 51-67-2
tyrosamine

: 4579-60-6
N-(p-hydroxyphenylethyl)-N-(3-hydroxy-4-methoxybenzyl)amine

Guidance literature:: isovanillin; tyrosamine; In toluene; butan-1-ol; for 4h; Heating / reflux;

With sodium tetrahydroborate; In methanol; at 0 ℃; for 4h;

Reference yield:

: 102686-18-0
5-{[(E)-2-(4-Hydroxy-phenyl)-ethylimino]-methyl}-2-methoxy-phenol

: 4579-60-6
N-(p-hydroxyphenylethyl)-N-(3-hydroxy-4-methoxybenzyl)amine

Guidance literature:: With sodium tetrahydroborate; In methanol; for 3h; Yield given; Ambient temperature;
DOI:10.1002/jhet.5570250639

Reference yield:

: 621-59-0
isovanillin

: 4579-60-6
N-(p-hydroxyphenylethyl)-N-(3-hydroxy-4-methoxybenzyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1.) molecular sieves, r.t., overnight

2: sodium borohydride / methanol / 3 h / Ambient temperature

With sodium tetrahydroborate; In methanol;
DOI:10.1002/jhet.5570250639