Benzeneheptanal, 4-octyl-

Base Information

• Chemical Name: Benzeneheptanal, 4-octyl-
• CAS No.: 873936-21-1
• Molecular Formula: C21H34O
• Molecular Weight: 302.5
• Mol file: 873936-21-1.mol

Synonyms:

Chemical Property of Benzeneheptanal, 4-octyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzeneheptanal, 4-octyl-

There total 5 articles about Benzeneheptanal, 4-octyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

7-(4-octylphenyl)-heptanol (86026-34-8) → 7-(4-octyl-phenyl)-heptanal (873936-21-1)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane;

DOI:10.1016/j.bmcl.2005.08.096

Reference yield:

7-(4-octyl-phenyl)-7-oxo-heptanoic acid (873936-20-0) → 7-(4-octyl-phenyl)-heptanal (873936-21-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 87 percent / aq. N₂H₄; KOH; ethanediol / microwave irradiation

2: 78 percent / BH₃*THF

3: 95 percent / PCC / CH₂Cl₂

With potassium hydroxide; borane-THF; hydrazine hydrate; ethylene glycol; pyridinium chlorochromate; In dichloromethane;

DOI:10.1016/j.bmcl.2005.08.096

Reference yield:

7-(4-octyl-phenyl)-heptanoic acid → 7-(4-octyl-phenyl)-heptanal (873936-21-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / BH₃*THF

2: 95 percent / PCC / CH₂Cl₂

With borane-THF; pyridinium chlorochromate; In dichloromethane;

DOI:10.1016/j.bmcl.2005.08.096

upstream raw materials:

7-(4-octylphenyl)-heptanol

7-(4-octyl-phenyl)-7-oxo-heptanoic acid

Octylbenzene

pimelic acid anhydride

Downstream raw materials:

4-benzyloxymethyl-2-[6-(4-octyl-phenyl)-hexyl]-[1,3]dioxolane