1-Piperidinecarboxylic acid, 3-[[3,4-dihydro-4-(3-methoxypropyl)-2H-1,4-benzoxazin-6-yl]methoxy]-5- hydroxy-4-(4-methoxyphenyl)-, phenylmethyl ester, (3R,4S,5S)-

Base Information

• Chemical Name: 1-Piperidinecarboxylic acid, 3-[[3,4-dihydro-4-(3-methoxypropyl)-2H-1,4-benzoxazin-6-yl]methoxy]-5- hydroxy-4-(4-methoxyphenyl)-, phenylmethyl ester, (3R,4S,5S)-
• CAS No.: 873945-56-3
• Molecular Formula: C33H40N2O7
• Molecular Weight: 576.69

Synonyms:

Chemical Property of 1-Piperidinecarboxylic acid, 3-[[3,4-dihydro-4-(3-methoxypropyl)-2H-1,4-benzoxazin-6-yl]methoxy]-5- hydroxy-4-(4-methoxyphenyl)-, phenylmethyl ester, (3R,4S,5S)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-Piperidinecarboxylic acid, 3-[[3,4-dihydro-4-(3-methoxypropyl)-2H-1,4-benzoxazin-6-yl]methoxy]-5- hydroxy-4-(4-methoxyphenyl)-, phenylmethyl ester, (3R,4S,5S)-

There total 3 articles about 1-Piperidinecarboxylic acid, 3-[[3,4-dihydro-4-(3-methoxypropyl)-2H-1,4-benzoxazin-6-yl]methoxy]-5- hydroxy-4-(4-methoxyphenyl)-, phenylmethyl ester, (3R,4S,5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3S,4S,5R)-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidin-3-ol (873945-55-2) + benzyl chloroformate (501-53-1,94274-21-2) → (3S,4S,5R)-3-hydroxy-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1-carboxylic acid benzyl ester (873945-56-3)

Guidance literature:

With sodium carbonate; In water; ethyl acetate; at 0 - 20 ℃; for 8h;

Reference yield:

benzyl (3R,4R,5S)-3-hydroxy-4-(4-methoxyphenyl)-5-triisopropylsilanyloxypiperidine-1-carboxylate (873945-60-9) → (3S,4S,5R)-3-hydroxy-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1-carboxylic acid benzyl ester (873945-56-3)

Guidance literature:

Reference yield:

→ (3S,4S,5R)-3-hydroxy-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1-carboxylic acid benzyl ester (873945-56-3)

Guidance literature:

upstream raw materials:

(3S,4S,5R)-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidin-3-ol

benzyl chloroformate

benzyl (3R,4R,5S)-3-hydroxy-4-(4-methoxyphenyl)-5-triisopropylsilanyloxypiperidine-1-carboxylate

Downstream raw materials:

(3S,4R,5R)-3-((S)-2-benzyloxycarbonylamino-3-methyl-butyryloxy)-4-(4-methoxyphenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]piperidine-1-carboxylic acid benzyl ester

benzyl (3S,4R,5R)-3((S)-3-benzyloxy-2-hydroxypropoxy)-4-(4-methoxyphenyl)-5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]piperidine-1-carboxylate

3-dimethylcarbamoyloxy-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1-carboxylic acid benzyl ester

3-(4-chlorophenoxy)-4-(4-methoxy-phenyl)-5-[4-(3-methoxy-propyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-piperidine-1-carboxylic acid benzyl ester

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