9-Tridecenoic acid, 13-(4-benzoylphenyl)-, (2S)-2,3-dihydroxypropyl ester, (9Z)-

Base Information

Chemical Name:9-Tridecenoic acid, 13-(4-benzoylphenyl)-, (2S)-2,3-dihydroxypropyl ester, (9Z)-
CAS No.:874140-90-6
Molecular Formula:C29H38O5
Molecular Weight:466.618
Hs Code.:

Synonyms:

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Chemical Property of 9-Tridecenoic acid, 13-(4-benzoylphenyl)-, (2S)-2,3-dihydroxypropyl ester, (9Z)-

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Technology Process of 9-Tridecenoic acid, 13-(4-benzoylphenyl)-, (2S)-2,3-dihydroxypropyl ester, (9Z)-

There total 7 articles about 9-Tridecenoic acid, 13-(4-benzoylphenyl)-, (2S)-2,3-dihydroxypropyl ester, (9Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874140-86-0
4-(13-hydrohytridec-4-ynyl)benzophenone

: 874140-90-6
1-((Z)-13-(4-benzoylphenyl)-9-tridecenoyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / hydrogen / Lindlar catalyst / methanol

2: 87 percent / PDC / dimethylformamide / 48 h / 20 °C

3: 92 percent / DCC; DMAP / CH₂Cl₂ / 40 h / 20 °C

4: 73 percent / hydrochloric acid / dioxane / 4 h / 20 °C

With hydrogenchloride; dmap; dipyridinium dichromate; hydrogen; dicyclohexyl-carbodiimide; Lindlar's catalyst; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052030w

Reference yield:

: 874140-85-9
4-(13-(tetrahydro-2H-pyran-2-yloxy)tridec-4-ynyl)benzophenone

: 874140-90-6
1-((Z)-13-(4-benzoylphenyl)-9-tridecenoyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / PPTS / methanol / 3 h / Heating

2: 97 percent / hydrogen / Lindlar catalyst / methanol

3: 87 percent / PDC / dimethylformamide / 48 h / 20 °C

4: 92 percent / DCC; DMAP / CH₂Cl₂ / 40 h / 20 °C

5: 73 percent / hydrochloric acid / dioxane / 4 h / 20 °C

With hydrogenchloride; dmap; dipyridinium dichromate; hydrogen; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; Lindlar's catalyst; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052030w

Reference yield:

: 19754-58-6
2-dec-9-ynyloxy-tetrahydro-pyran

: 874140-90-6
1-((Z)-13-(4-benzoylphenyl)-9-tridecenoyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

1.2: 1.85 g / CuI / tetrahydrofuran; hexane / 20 °C

2.1: 9-BBN / tetrahydrofuran / -15 - 20 °C

2.2: 66 percent / K₃PO₄ / Pd(PPh₃)4 / dimethylformamide; tetrahydrofuran / 2 h / Heating

3.1: 93 percent / PPTS / methanol / 3 h / Heating

4.1: 97 percent / hydrogen / Lindlar catalyst / methanol

5.1: 87 percent / PDC / dimethylformamide / 48 h / 20 °C

6.1: 92 percent / DCC; DMAP / CH₂Cl₂ / 40 h / 20 °C

7.1: 73 percent / hydrochloric acid / dioxane / 4 h / 20 °C

With hydrogenchloride; dmap; dipyridinium dichromate; 9-borabicyclo[3.3.1]nonane dimer; n-butyllithium; hydrogen; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; Lindlar's catalyst; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; 2.2: Suzuki reaction;
DOI:10.1021/jo052030w