2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one

Base Information

Chemical Name:2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one
CAS No.:87427-90-5
Molecular Formula:C10H10N2O3
Molecular Weight:206.201
Hs Code.:
DSSTox Substance ID:DTXSID60538415
Wikidata:Q82413800

Synonyms:2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one;87427-90-5;DTXSID60538415;AKOS000277810

Suppliers and Price of 2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:206.06914219
Heavy Atom Count:15
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=NNC(=O)CO2

Technology Process of 2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one

There total 2 articles about 2-(4-Methoxyphenyl)-4H-1,3,4-oxadiazin-5(6H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 50677-25-3
PCM-0102115

: 87427-90-5
2-(4-Methoxy-phenyl)-4H-[1,3,4]oxadiazin-5-one

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 60 ℃; for 20h;
DOI:10.1016/0223-5234(88)90141-9

Reference yield:

: 3290-99-1
4-methoxybenzoic acid hydrazide

: 87427-90-5
2-(4-Methoxy-phenyl)-4H-[1,3,4]oxadiazin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ethyl acetate / 0.5 h / Heating

2: 31 percent / NaHCO₃ / dimethylformamide / 20 h / 60 °C

With sodium hydrogencarbonate; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90141-9