Technology Process of Phosphinic acid, 2-pentenyl-, phenylmethyl ester
There total 1 articles about Phosphinic acid, 2-pentenyl-, phenylmethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium phosphinate; hexamethyldisilazane / CH2Cl2 / 20 °C
2: dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / tetrahydrofuran / 20 °C
With
dmap; ammonium hypophosphite; dicyclohexyl-carbodiimide; 1,1,1,3,3,3-hexamethyl-disilazane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm050922i
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
toluene;
at 20 ℃;
for 72h;
DOI:10.1021/jm050922i
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 47 percent / BF3*Et2O / toluene / 72 h / 20 °C
2: 76 percent / trifluoroacetic acid / CH2Cl2 / 0.25 h / 20 °C
With
boron trifluoride diethyl etherate; trifluoroacetic acid;
In
dichloromethane; toluene;
DOI:10.1021/jm050922i
