2-Oxazolidinone, 3-(4-methoxyphenyl)-4,5-bis(methylene)-

Base Information

Chemical Name:2-Oxazolidinone, 3-(4-methoxyphenyl)-4,5-bis(methylene)-
CAS No.:874304-60-6
Molecular Formula:C12H11NO3
Molecular Weight:217.224
Hs Code.:

Synonyms:

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Chemical Property of 2-Oxazolidinone, 3-(4-methoxyphenyl)-4,5-bis(methylene)-

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Technology Process of 2-Oxazolidinone, 3-(4-methoxyphenyl)-4,5-bis(methylene)-

There total 1 articles about 2-Oxazolidinone, 3-(4-methoxyphenyl)-4,5-bis(methylene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 5416-93-3
4-Methoxyphenyl isocyanate

: 431-03-8
dimethylglyoxal

: 874304-60-6
3-(4-anisyl)-4,5-dimethylene-1,3-oxazolidin-2-one

Guidance literature:: With lithium carbonate; triethylamine; In 1,4-dioxane; at 20 ℃; for 24h;
DOI:10.1055/s-2007-983741

Reference yield: 93.0%

: 874304-60-6
3-(4-anisyl)-4,5-dimethylene-1,3-oxazolidin-2-one

: 107-02-8,25068-14-8
acrolein

: 934196-86-8
6-formyl-3-(4-methoxyphenyl)-2,3,4,5,6,7-hexahydrobenzoxazol-2-one

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 0.25h;
DOI:10.1055/s-2007-983741

Reference yield: 63.0%

: 874304-60-6
3-(4-anisyl)-4,5-dimethylene-1,3-oxazolidin-2-one

: chlorobis(cyclooctene)-iridium(I) dimer

: 17567-17-8
potassium hydridotris(3,5-dimethylpyrazolyl)borate

: [(hydrotris(3,5-dimethylpyrazolyl)borate)Ir(CH₂=C(N(4-CH₃OC₆H₄)C(O)O)C=CH₂)]

Guidance literature:: In tetrahydrofuran; (N2 or Ar, Schlenk) to a suspn. of complex in THF cooled to -20°Cwas added oxazolidinine-compound, the mixt. was stirred for 20 min, bor ate-compound in THF was added, the mixt. was stirred for 4 h at 20°C; the solvent was removed under vac., extd. with a mixt. of CH2Cl2-diethylether, centrifuged, cooled to -20°C;
DOI:10.1021/om050582z