4-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine

Base Information

• Chemical Name: 4-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine
• CAS No.: 42833-31-8
• Molecular Formula: C10H18N2O
• Molecular Weight: 182.2627
• NSC Number: 162076
• DSSTox Substance ID: DTXSID90303794
• Nikkaji Number: J2.005.234A
• Wikidata: Q82049257
• Mol file: 42833-31-8.mol

Synonyms:42833-31-8;4-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine;NSC162076;4-(1-methyl-3,6-dihydro-2H-pyridin-4-yl)morpholine;SCHEMBL1967895;4-(1-methyl-1,2,3,6-tetrahydro-4-pyridinyl)morpholine;DTXSID90303794;DCFOWKDNANGCTA-UHFFFAOYSA-N;MFCD00180790;AKOS006275200;NSC-162076;FT-0725286;12G-915;1-N-Methyl-4-morpholin-4-yl-1,2,5,6-tetrahydropyridine

Chemical Property of 4-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine

Chemical Property:

• Vapor Pressure: 0.00135mmHg at 25°C
• Boiling Point: 297.4°Cat760mmHg
• Flash Point: 90.4°C
• Density: 1.065g/cm³
• XLogP3: 0.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 182.141913202
• Heavy Atom Count: 13
• Complexity: 197

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1CCC(=CC1)N2CCOCC2

Technology Process of 4-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine

There total 2 articles about 4-(1-Methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

morpholine (110-91-8,99108-56-2) + 1-Methyl-4-piperidone (1445-73-4) → 4-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine (42833-31-8)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 16h; Heating;

DOI:10.1002/ardp.19853180714

Reference yield:

→ 4-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine (42833-31-8)

Guidance literature:

1-Methyl-piperidon-(4), Morpholin (1.1 Mol), sehr wenig p-Toluolsulfonsaeure, Sieden;

Reference yield: 92.0%

4-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine (42833-31-8) + 3-Benzyliden-2,3-dihydro-4H-1-benzothiopyran-4-on-1,1-dioxid (101001-24-5) → 7,7a,8,9,10,11-Hexahydro-9-methyl-11a-morpholino-7-phenyl-6H,7H-<1>benzothiopyrano<3,4'-5,6>pyrano<3,2-c>pyridin-5,5-dioxid (93628-28-5)

Guidance literature:

In methanol; at 40 ℃; for 15h;

DOI:10.1002/ardp.19843171010

upstream raw materials:

morpholine

1-Methyl-4-piperidone

Downstream raw materials:

4-[N-(4-chloro-benzenesulfonyl)-1-methyl-pyrrolidine-3-carboximidoyl]-morpholine

6-methyl-8a-morpholin-4-yl-2,3-diphenyl-2,3,4a,5,6,7,8,8a-octahydro-tetrazolo[5',1':2,3]thiazolo[4,5-c]pyridine

6-methyl-8a-morpholin-4-yl-1-phenyl-3-phenylazo-(4ar,8ac)-4a,5,6,7,8,8a-hexahydro-1H-pyrido[4,3-e][1,3,4]thiadiazine

1-methyl-4-morpholin-4-yl-1,2,3,6-tetrahydro-pyridine-3,5-dicarboxylic acid dianilide

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