2-Benzofuranpropanoic acid, 3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester

Base Information

Chemical Name:2-Benzofuranpropanoic acid, 3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester
CAS No.:874774-05-7
Molecular Formula:C36H47N3O8
Molecular Weight:649.784
Hs Code.:

2-Benzofuranpropanoic acid,
3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen
ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester

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Chemical Property of 2-Benzofuranpropanoic acid, 3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester

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Technology Process of 2-Benzofuranpropanoic acid, 3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester

There total 1 articles about 2-Benzofuranpropanoic acid, 3-[[(2S)-1-[(2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-oxo-5-[[(phen ylmethoxy)carbonyl]amino]pentyl]-2-pyrrolidinyl]methyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 874773-95-2
3-(3-pyrrolidin-2-ylmethyl-benzofuran-2-yl)-propionic acid ethyl ester

: 874774-05-7
3-{3-[1-(5-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-pentanoyl)-pyrrolidin-2-ylmethyl]-benzofuran-2-yl}-propionic acid ethyl ester

Guidance literature:: Boc-Orn(Z)-OH; With 4-methyl-morpholine; HATU; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 0.166667h;

3-(3-pyrrolidin-2-ylmethyl-benzofuran-2-yl)-propionic acid ethyl ester; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 16h;

Reference yield: 100.0%

: 874774-05-7
3-{3-[1-(5-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-pentanoyl)-pyrrolidin-2-ylmethyl]-benzofuran-2-yl}-propionic acid ethyl ester

: 874774-07-9
3-{3-[1-(5-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-pentanoyl)-pyrrolidin-2-ylmethyl]-benzofuran-2-yl}-propionic acid

Guidance literature:: 3-{3-[1-(5-benzyloxycarbonylamino-2-tert-butoxycarbonylamino-pentanoyl)-pyrrolidin-2-ylmethyl]-benzofuran-2-yl}-propionic acid ethyl ester; With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 2.5h; Heating / reflux;

With hydrogenchloride; In ethyl acetate;