Technology Process of L-Serine, 3-ethoxy-O-ethyl-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-
There total 6 articles about L-Serine, 3-ethoxy-O-ethyl-N-[(9H-fluoren-9-ylmethoxy)carbonyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hypochlorite; disodium hydrogenphosphate; sodium dihydrogenphosphate;
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite;
In
water; acetonitrile;
at 35 ℃;
DOI:10.1021/ol052623t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94 percent / CSA / ethanol / 10 h / 85 °C
2: 87 percent / Na2HPO4; NaH2PO4; NaOCl / NaClO2; TEMPO / acetonitrile; H2O / 35 °C
With
sodium hypochlorite; disodium hydrogenphosphate; sodium dihydrogenphosphate; camphor-10-sulfonic acid;
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite;
In
ethanol; water; acetonitrile;
DOI:10.1021/ol052623t
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 99 percent / NaHCO3 / H2O; dioxane / cooling
2: 98 percent / BF3*Et2O / acetone / 3 h / 20 °C
3: 9.56 g / LiBH4 / diethyl ether; toluene / 20 °C
4: 92 percent / NaBr; NaOCl; NaHCO3 / TEMPO / ethyl acetate; toluene; H2O / cooling
5: 94 percent / CSA / ethanol / 10 h / 85 °C
6: 87 percent / Na2HPO4; NaH2PO4; NaOCl / NaClO2; TEMPO / acetonitrile; H2O / 35 °C
With
sodium hypochlorite; disodium hydrogenphosphate; sodium dihydrogenphosphate; lithium borohydride; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium hydrogencarbonate; sodium bromide;
2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium chlorite;
In
1,4-dioxane; diethyl ether; ethanol; water; ethyl acetate; acetone; toluene; acetonitrile;
DOI:10.1021/ol052623t