Technology Process of Methanone, [6-hydroxy-5-(2-propenyl)-2-naphthalenyl]phenyl-
There total 1 articles about Methanone, [6-hydroxy-5-(2-propenyl)-2-naphthalenyl]phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: KOH / dimethylsulfoxide / 0.5 h / 20 °C
1.2: 80 percent / dimethylsulfoxide / 2 h / 20 °C
2.1: 95 percent / 1,2-dichloro-benzene / 0.25 h / 250 °C / microwave irradiation
With
potassium hydroxide;
In
dimethyl sulfoxide; 1,2-dichloro-benzene;
2.1: Claisen rearrangement;
DOI:10.1021/jm0510373
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 2h;
under 2280 Torr;
DOI:10.1021/jm0510373
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 97 percent / H2 / Pd/C / ethyl acetate / 2 h / 2280 Torr
2: K2CO3; KI / dimethylformamide / 110 °C
3: K2CO3; KI / acetonitrile / Heating
4: aq. LiOH / methanol / Heating
With
lithium hydroxide; hydrogen; potassium carbonate; potassium iodide;
palladium on activated charcoal;
In
methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm0510373
