Benzenethiol, 2-bromo-4-(trifluoromethoxy)-

Base Information

Chemical Name:Benzenethiol, 2-bromo-4-(trifluoromethoxy)-
CAS No.:875143-35-4
Molecular Formula:C7H4BrF3OS
Molecular Weight:273.073
Hs Code.:

Synonyms:

Suppliers and Price of Benzenethiol, 2-bromo-4-(trifluoromethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of Benzenethiol, 2-bromo-4-(trifluoromethoxy)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of Benzenethiol, 2-bromo-4-(trifluoromethoxy)-

There total 1 articles about Benzenethiol, 2-bromo-4-(trifluoromethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 175278-17-8
2-bromo-4-trifluoromethoxyaniline

: 875143-35-4
2-bromo-4-trifluoromethoxythiophenol

Guidance literature:: 2-bromo-4-trifluoromethoxyaniline; With hydrogenchloride; sodium nitrite; at 0 ℃;

With potassium xanthate; at 70 ℃; for 45h;
DOI:10.1021/jm051059p

Reference yield: 90.0%

: 875143-35-4
2-bromo-4-trifluoromethoxythiophenol

: (1R/S,2R/S)-(2-{[(cyanomethyl)amino]carbonyl}-cyclohexyl)methyl-4-methylbenzenesulfonate

: 2-({[2-bromo-4-(trifluoromethoxy)phenyl]thio}methyl)-N-(cyanomethyl)cyclohexanecarboxamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 22h;
DOI:10.1021/jm051059p

Reference yield:

: 875143-35-4
2-bromo-4-trifluoromethoxythiophenol

: C₁₇H₁₈⁽³⁾HF₃N₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃ / dimethylformamide / 22 h / 20 °C

2: aq. NaHCO₃; Oxone(R) / methanol; ethyl acetate / 1 h / 40 °C

3: Et₃N; tritium gas / Pd/C / tetrahydrofuran / 598 Torr

With tritium; oxone; sodium hydrogencarbonate; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm051059p