5-Methylpicolinimidamide hydrochloride

Base Information

• Chemical Name: 5-Methylpicolinimidamide hydrochloride
• CAS No.: 875293-96-2
• Molecular Formula: C7H9N3.ClH
• Molecular Weight: 171.62700
• Hs Code.: 2933399090
• DSSTox Substance ID: DTXSID60704279
• Mol file: 875293-96-2.mol

Synonyms:5-methylpicolinimidamide hydrochloride;875293-96-2;5-methylpyridine-2-carboximidamide;hydrochloride;5-Methyl-pyridine-2-carboxamidine;5-Methylpicolinimidamidehydrochloride;SCHEMBL2972454;DTXSID60704279;MFCD12755541;AKOS015844066;5-Methyl-pyridine-2-carboxamidine HCl;AS-6303;CS-0314495;5-Methyl-pyridine-2-carboxamidine hydrochloride;W19131;A862543;5-METHYLPYRIDINE-2-CARBOXIMIDAMIDE HYDROCHLORIDE;5-Methylpyridine-2-carboximidamide--hydrogen chloride (1/1)

Chemical Property of 5-Methylpicolinimidamide hydrochloride

Chemical Property:

• PSA: 62.76000
• LogP: 2.27610
• Storage Temp.: Sealed in dry,Room Temperature
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 171.0563250
• Heavy Atom Count: 11
• Complexity: 133

Purity/Quality:

≥95% ^*data from raw suppliers

5-methylpicolinimidamidehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CN=C(C=C1)C(=N)N.Cl

Technology Process of 5-Methylpicolinimidamide hydrochloride

There total 2 articles about 5-Methylpicolinimidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methylpicolinonitrile (1620-77-5) → 5-methylpyridine-2-carboxamidine hydrochloride (875293-96-2)

Guidance literature:

5-methylpicolinonitrile; 2; With sodium methylate; In methanol; at 20 ℃; for 12h;

With ammonium chloride; In methanol; for 3h; Reflux;

Reference yield:

→ 5-methylpyridine-2-carboxamidine hydrochloride (875293-96-2)

Guidance literature:

Reference yield:

1-(4-methylsulfonylphenyl)piperidin-4-one (116248-04-5) + 5-methylpyridine-2-carboxamidine hydrochloride (875293-96-2) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 2-(5-methyl-2-pyridyl)-6-(4-methylsulfonylphenyl)-7,8-dihydro-5H-pyrido[4,3-d]pyrimidine

Guidance literature:

1-(4-methylsulfonylphenyl)piperidin-4-one; N,N-dimethyl-formamide dimethyl acetal; In acetonitrile; at 90 ℃; for 2h;

5-methylpyridine-2-carboxamidine hydrochloride; With potassium carbonate; In ethanol; at 90 ℃;

upstream raw materials:

5-methylpicolinonitrile

Refernces

• 1、 -. "2-(PYRIDIN-2-YL)-PYRIMIDINES AND THEIR USE FOR CONTROLLING PATHOGENIC FUNGI". Page/Page column 48. . Retrieved 2010/02/15.