2-chloro-7-ethyl-12,13-dimethoxy-5,9,10,14b-tetrahydroisoquino[2,1-d][1,4]benzodiazepin-6(7H)-one

Base Information

• Chemical Name: 2-chloro-7-ethyl-12,13-dimethoxy-5,9,10,14b-tetrahydroisoquino[2,1-d][1,4]benzodiazepin-6(7H)-one
• CAS No.: 102395-73-3
• Molecular Formula: C₂₁H₂₃ClN₂O₃
• Molecular Weight: 386.878

Synonyms:Isoquino[2,1-d][1,4]benzodiazepin-6(7H)-one,2-chloro-7-ethyl-5,9,10,14b-tetrahydro-12,13-dimethoxy- (9CI)

Chemical Property of 2-chloro-7-ethyl-12,13-dimethoxy-5,9,10,14b-tetrahydroisoquino[2,1-d][1,4]benzodiazepin-6(7H)-one

Chemical Property:

• Vapor Pressure: 5.47E-11mmHg at 25°C
• Boiling Point: 521.8°Cat760mmHg
• Flash Point: 269.4°C
• Density: 1.31g/cm³

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-chloro-7-ethyl-12,13-dimethoxy-5,9,10,14b-tetrahydroisoquino[2,1-d][1,4]benzodiazepin-6(7H)-one

There total 2 articles about 2-chloro-7-ethyl-12,13-dimethoxy-5,9,10,14b-tetrahydroisoquino[2,1-d][1,4]benzodiazepin-6(7H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chlor-7-ethyl-12,13-dimethoxy-6-oxo-9,10-dihydroisochino<2,1-d><1,4>-benzodiazepiniumbromid (74099-05-1) → (7R,13bS)-12-Chloro-7-ethyl-2,3-dimethoxy-5,6,9,13b-tetrahydro-6a,9-diaza-benzo[6,7]cyclohepta[1,2-a]naphthalen-8-one (74099-03-9,74099-04-0,82838-37-7,82863-41-0,102395-73-3) + (7S,13bS)-12-Chloro-7-ethyl-2,3-dimethoxy-5,6,9,13b-tetrahydro-6a,9-diaza-benzo[6,7]cyclohepta[1,2-a]naphthalen-8-one (74099-03-9,74099-04-0,82838-37-7,82863-41-0,102395-73-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 3h; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1002/ardp.19803130208

Reference yield:

2-Chlor-7-ethyl-12,13-dimethoxy-6-oxo-9,10-dihydroisochino<2,1-d><1,4>-benzodiazepiniumbromid (74099-05-1) → (7R,13bS)-12-Chloro-7-ethyl-2,3-dimethoxy-5,6,9,13b-tetrahydro-6a,9-diaza-benzo[6,7]cyclohepta[1,2-a]naphthalen-8-one (74099-03-9,74099-04-0,82838-37-7,82863-41-0,102395-73-3) + (7S,13bS)-12-Chloro-7-ethyl-2,3-dimethoxy-5,6,9,13b-tetrahydro-6a,9-diaza-benzo[6,7]cyclohepta[1,2-a]naphthalen-8-one (74099-03-9,74099-04-0,82838-37-7,82863-41-0,102395-73-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 3h; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1002/ardp.19803130208

upstream raw materials:

2-Chlor-7-ethyl-12,13-dimethoxy-6-oxo-9,10-dihydroisochino<2,1-d><1,4>-benzodiazepiniumbromid

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