DI-SEC-OCTYLAMINE

Base Information

• Chemical Name: DI-SEC-OCTYLAMINE
• CAS No.: 5412-92-0
• Molecular Formula: C16H35 N
• Molecular Weight: 241.461
• Hs Code.: 2921199090
• Mol file: 5412-92-0.mol

Synonyms:Diheptylamine,1,1'-dimethyl- (6CI,7CI,8CI); Bis(1-methylheptyl)amine; NSC 6350

Chemical Property of DI-SEC-OCTYLAMINE

Chemical Property:

• Vapor Pressure: 0.00366mmHg at 25°C
• Melting Point: 14.62°C (estimate)
• Refractive Index: 1.4400 (estimate)
• Boiling Point: 281°Cat760mmHg
• Flash Point: 109.7°C
• PSA: 12.03000
• Density: 0.798g/cm³
• LogP: 5.68470

Purity/Quality:

97% ^*data from raw suppliers

DI-SEC-OCTYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DI-SEC-OCTYLAMINE

There total 4 articles about DI-SEC-OCTYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexyl-methyl-ketone (111-13-7) → rac-2-aminooctane (44855-57-4,693-16-3) + rac-octan-2-ol (4128-31-8,113301-48-7,4128-32-9) + bis(2-octyl)amine (5412-92-0)

Guidance literature:

With ammonia; hydrogen; In o-xylene; at 100 ℃; for 20h; Autoclave;

DOI:10.1002/cctc.201402996

Reference yield:

rac-octan-2-ol (4128-31-8,113301-48-7,4128-32-9) → rac-2-aminooctane (44855-57-4,693-16-3) + bis(2-octyl)amine (5412-92-0)

Guidance literature:

With ammonia; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 - 160 ℃; for 4h; under 3000.3 Torr; Sealed tube; Autoclave;

DOI:10.1021/cs3007473

Reference yield:

rac-octan-2-ol (4128-31-8,113301-48-7,4128-32-9) → rac-2-aminooctane (44855-57-4,693-16-3) + bis(2-octyl)amine (5412-92-0) + hexyl-methyl-ketone (111-13-7)

Guidance literature:

With ammonia; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 - 160 ℃; for 4h; under 3000.3 Torr; Sealed tube; Autoclave;

DOI:10.1021/cs3007473

upstream raw materials:

hexyl-methyl-ketone

rac-octan-2-ol

Refernces

• 1、 Shimizu, Ken-Ichi,Kon, Kenichi,Onodera, Wataru,Yamazaki, Hiroshi,Kondo, Junko N.. "Heterogeneous Ni catalyst for direct synthesis of primary amines from alcohols and ammonia". . p. 112 - 117. Retrieved 2013/03/29.