Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)-

Base Information

Chemical Name:Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)-
CAS No.:876065-69-9
Molecular Formula:C₂₂H₁₇NOS
Molecular Weight:343.449
Hs Code.:

Synonyms:

Suppliers and Price of Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)-

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Chemical Property of Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)-

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Technology Process of Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)-

There total 11 articles about Isoindolo[1,2-a]isoquinolin-8(6H)-one, 5,12b-dihydro-5-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 574-98-1
2-(2-bromoethyl)isoindoline-1,3-dione

: 876065-69-9
5,12b-dihydro-5-phenylthioisoindolo[1,2-a]isoquinolin-8(6H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / sodium methoxide / dimethylformamide / 48 h / 20 °C

2: 88 percent / diethyl ether; tetrahydrofuran / 20 °C

3: 89 percent / TFA; triethylsilane / CH₂Cl₂ / 4 h / 0 - 20 °C

4: 100 percent / m-CPBA / CH₂Cl₂ / 0.17 h / -60 - 20 °C

5: 100 percent / TFAA / CH₂Cl₂ / 0.5 h / 20 °C

With triethylsilane; sodium methylate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.10.017

Reference yield:

: 876065-67-7
2-(2-chloroethyl)-2,3-dihydro-3-phenylisoindol-1-one

: 876065-69-9
5,12b-dihydro-5-phenylthioisoindolo[1,2-a]isoquinolin-8(6H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / sodium methoxide / dimethylformamide / 12 h / 100 °C

2: 100 percent / m-CPBA / CH₂Cl₂ / 0.17 h / -60 - 20 °C

3: 100 percent / TFAA / CH₂Cl₂ / 0.5 h / 20 °C

With sodium methylate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.10.017

Reference yield:

: 876065-66-6
2,3-dihydro-3-phenyl-2-(2-phenylthioethyl)-isoindol-1-one

: 876065-69-9
5,12b-dihydro-5-phenylthioisoindolo[1,2-a]isoquinolin-8(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / m-CPBA / CH₂Cl₂ / 0.17 h / -60 - 20 °C

2: 100 percent / TFAA / CH₂Cl₂ / 0.5 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1016/j.tet.2005.10.017