dihydrovirginiamycin S1

Base Information

• Chemical Name: dihydrovirginiamycin S1
• CAS No.: 26549-61-1
• Molecular Formula: C₄₃H₅₁N₇O₁₀
• Molecular Weight: 825.919
• Mol file: 26549-61-1.mol

Synonyms:StaphylomycinS, 5-(4-hydroxy-L-pipecolic acid)- (8CI); Virginiamycin S1, 5-(4-hydroxy-L-2-piperidinecarboxylicacid)-;12H-Pyrido[2,1-f]pyrrolo[2,1-l][1,4,7,10,13,16]oxapentaazacyclononadecine,cyclic peptide deriv.; Dihydrostaphylomycin S; Dihydrovirginiamycin S1;Virginiamycin S1, dihydro-

Chemical Property of dihydrovirginiamycin S1

Chemical Property:

• Boiling Point: 1224.5±65.0 °C(Predicted)
• PKA: 3.52±0.35(Predicted)
• Density: 1.40±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of dihydrovirginiamycin S1

There total 3 articles about dihydrovirginiamycin S1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

Alloc-L-MePhe-OH + (2S,3R)-3-((S)-2-Amino-2-phenyl-acetoxy)-2-tert-butoxycarbonylamino-butyric acid allyl ester (793718-13-5) + 4-hydroxy-piperidine-1,2-dicarboxylic acid 2-tert-butyl ester 1-(9H-fluoren-9-ylmethyl) ester + Fmoc-Pro-OH (71989-31-6) → dihydrovirginiamycin S1 (26549-61-1,42116-61-0,42116-62-1)

Guidance literature:

Multistep reaction;

DOI:10.1002/chem.200400267

Reference yield:

cyclo-(γO)Pec-PhgO-((3'OH)Pic-)Thr-D-Abu-Pro-MePhe-O- (23152-29-6) → N-(3-hydroxy-pyridine-2-carbonyl)-Ls-threonyl->D-2-amino-butyryl->L-prolyl->N-methyl-L-phenylalanyl->(2S,4R)-4-hydroxy-piperidine-2-carbonyl->(S)-2-phenyl-glycine [1]3-lactone (26549-61-1,42116-61-0,42116-62-1) + dihydrovirginiamycin S1 (26549-61-1,42116-61-0,42116-62-1)

Guidance literature:

With sodium tetrahydroborate; acetic acid; In ethanol; Ambient temperature;

DOI:10.7164/antibiotics.30.141

Reference yield:

cyclo-(γO)Pec-PhgO-((3'OH)Pic-)Thr-D-Abu-Pro-MePhe-O- (23152-29-6) → N-(3-hydroxy-pyridine-2-carbonyl)-Ls-threonyl->D-2-amino-butyryl->L-prolyl->N-methyl-L-phenylalanyl->(2S,4R)-4-hydroxy-piperidine-2-carbonyl->(S)-2-phenyl-glycine [1]3-lactone (26549-61-1,42116-61-0,42116-62-1) + dihydrovirginiamycin S1 (26549-61-1,42116-61-0,42116-62-1)

Guidance literature:

With sodium tetrahydroborate; acetic acid; In ethanol; Ambient temperature;

DOI:10.7164/antibiotics.30.141

upstream raw materials:

cyclo-(γO)Pec-PhgO-((3'OH)Pic-)Thr-D-Abu-Pro-MePhe-O-

(2S,3R)-3-((S)-2-Amino-2-phenyl-acetoxy)-2-tert-butoxycarbonylamino-butyric acid allyl ester

Fmoc-Pro-OH

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