1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Base Information

Chemical Name:1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone
CAS No.:34790-06-2
Molecular Formula:C11H12 Cl2 N2 O
Molecular Weight:259.135
Hs Code.:2933599090
Mol file:34790-06-2.mol

Synonyms:1-(3,4-Dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Suppliers and Price of 1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(3,4-DICHLOROBENZYL)-3,4,5,6-TETRAHYDRO-2(1H)-PYRIMIDONE 95.00%
5MG
$ 505.25

Total 3 raw suppliers

Chemical Property of 1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Chemical Property:

Vapor Pressure:5.9E-09mmHg at 25°C
Boiling Point:468.6°Cat760mmHg
Flash Point:237.2°C
PSA：35.83000
Density:1.347g/cm³
LogP:2.48660

Purity/Quality:

99% ^*data from raw suppliers

1-(3,4-DICHLOROBENZYL)-3,4,5,6-TETRAHYDRO-2(1H)-PYRIMIDONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

There total 2 articles about 1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 34790-05-1
1-(3,4-dichlorobenzyl)-2(1H)-pyrimidone

: 34790-06-2
1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; for 7h; under 2280 - 3040 Torr;
DOI:10.1002/jps.2600691020

Reference yield:

: 102-47-6
3,4-Dichlorophenylmethyl chloride

: 34790-06-2
1-(3,4-dichlorobenzyl)-3,4,5,6-tetrahydro-2(1H)-pyrimidone

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / potassium carbonate, potassium iodide / methanol / 24 h / Heating

2: 77 percent / H₂ / platinic oxide / methanol / 7 h / 2280 - 3040 Torr

With hydrogen; potassium carbonate; potassium iodide; platinum(IV) oxide; In methanol;
DOI:10.1002/jps.2600691020