[1,1'-Binaphthacene]-4,4'-dicarboxylicacid,3,3'-diethyl-1,1',2,2',3,3',4,4',6,6',11,11'-dodecahydro-3,3',10,10',12,12'-hexahydroxy-6,6',11,11'-tetraoxo-,dimethyl ester (9CI)

Base Information

• Chemical Name: [1,1'-Binaphthacene]-4,4'-dicarboxylicacid,3,3'-diethyl-1,1',2,2',3,3',4,4',6,6',11,11'-dodecahydro-3,3',10,10',12,12'-hexahydroxy-6,6',11,11'-tetraoxo-,dimethyl ester (9CI)
• CAS No.: 64040-81-9
• Molecular Formula: C₄₄H₃₈O₁₄
• Molecular Weight: 790.777

Synonyms:AntibioticMA 144E1

Chemical Property of [1,1'-Binaphthacene]-4,4'-dicarboxylicacid,3,3'-diethyl-1,1',2,2',3,3',4,4',6,6',11,11'-dodecahydro-3,3',10,10',12,12'-hexahydroxy-6,6',11,11'-tetraoxo-,dimethyl ester (9CI)

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SDS file from LookChem

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Technology Process of [1,1'-Binaphthacene]-4,4'-dicarboxylicacid,3,3'-diethyl-1,1',2,2',3,3',4,4',6,6',11,11'-dodecahydro-3,3',10,10',12,12'-hexahydroxy-6,6',11,11'-tetraoxo-,dimethyl ester (9CI)

There total 1 articles about [1,1'-Binaphthacene]-4,4'-dicarboxylicacid,3,3'-diethyl-1,1',2,2',3,3',4,4',6,6',11,11'-dodecahydro-3,3',10,10',12,12'-hexahydroxy-6,6',11,11'-tetraoxo-,dimethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

d,l-Bi(3,5,5-trimethyl-2-oxomorpholin-3-yl) (53153-53-0) + aclacinomycin A (57576-44-0,64520-15-6,77448-81-8,79617-46-2) → 3,5,5-trimethyl-2-oxomorpholine (57765-62-5) + 5,6-dihydro-3,5,5-trimethyl-1,4-oxazin-2-one (53153-46-1) + methyl 9(R,S)-ethyl-4,6,9(R,S)-trihydroxy-5,12-dioxo-7,8,9,10-tetrahydronaphthacene-10(R,S)-carboxylate (78821-96-2) + bi(7-deoxyaklavinon-7-yl) (64040-81-9)

Guidance literature:

With Trizma-buffer; In methanol; for 24h; Ambient temperature;

DOI:10.1021/ja00316a049

Reference yield: 40.0%

d,l-Bi(3,5,5-trimethyl-2-oxomorpholin-3-yl) (53153-53-0) + bi(7-deoxyaklavinon-7-yl) (64040-81-9) → 3,5,5-trimethyl-2-oxomorpholine (57765-62-5) + 5,6-dihydro-3,5,5-trimethyl-1,4-oxazin-2-one (53153-46-1) + methyl 9(R,S)-ethyl-4,6,9(R,S)-trihydroxy-5,12-dioxo-7,8,9,10-tetrahydronaphthacene-10(R,S)-carboxylate (78821-96-2)

Guidance literature:

With tris hydrochloride; 2-amino-2-hydroxymethyl-1,3-propanediol; In methanol; for 24h; Ambient temperature;

DOI:10.1021/ja00316a049

upstream raw materials:

d,l-Bi(3,5,5-trimethyl-2-oxomorpholin-3-yl)

aclacinomycin A

Downstream raw materials:

3,5,5-trimethyl-2-oxomorpholine

5,6-dihydro-3,5,5-trimethyl-1,4-oxazin-2-one

methyl 9(R,S)-ethyl-4,6,9(R,S)-trihydroxy-5,12-dioxo-7,8,9,10-tetrahydronaphthacene-10(R,S)-carboxylate

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